4-Benzyl 1-Methyl 2-nitroterephthalate

Base Information

• Chemical Name: 4-Benzyl 1-Methyl 2-nitroterephthalate
• CAS No.: 402925-14-8
• Molecular Formula: C16H13NO6
• Molecular Weight: 315.282
• Hs Code.: 2917399090
• Mol file: 402925-14-8.mol

Synonyms:4-Benzyl 1-methyl 2-nitroterephthalate;benzyl 3-nitro-4-methoxycarbonylbenzoate;

Chemical Property of 4-Benzyl 1-Methyl 2-nitroterephthalate

Chemical Property:

• Boiling Point: 461.7±30.0 °C(Predicted)
• PSA: 98.42000
• Density: 1.326±0.06 g/cm3(Predicted)
• LogP: 3.26160
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Benzyl1-methyl2-nitroterephthalate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Benzyl 1-Methyl 2-nitroterephthalate

There total 1 articles about 4-Benzyl 1-Methyl 2-nitroterephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4-(methoxycarbonyl)-3-nitrobenzoic acid (35092-89-8) + 2-bromo-4-hydroxybenzoic acid (28547-28-6) + benzyl bromide (100-39-0) → benzyl 3-nitro-4-methoxycarbonylbenzoate (402925-14-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield: 61.0%

benzyl 3-nitro-4-methoxycarbonylbenzoate (402925-14-8) + iron (7439-89-6) → 1-methyl-4-benzyl 2-aminoterephthalate (330807-53-9)

Guidance literature:

With ammonium chloride; In water; isopropyl alcohol;

upstream raw materials:

4-(methoxycarbonyl)-3-nitrobenzoic acid

2-bromo-4-hydroxybenzoic acid

benzyl bromide

Downstream raw materials:

1-methyl-4-benzyl 2-aminoterephthalate