N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-D-ribofuranosylamine

Base Information

Chemical Name:N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-D-ribofuranosylamine
CAS No.:157306-00-8
Molecular Formula:C₁₆H₂₅NO₈
Molecular Weight:359.376
Hs Code.:
Mol file:157306-00-8.mol

Synonyms:Furo[3,4-d]-1,3-dioxole,propanedioic acid deriv.

Suppliers and Price of N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-D-ribofuranosylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-D-ribofuranosylamine

Chemical Property:

Vapor Pressure:4.92E-10mmHg at 25°C
Boiling Point:451.1°Cat760mmHg
PKA:14.14±0.10(Predicted)
Flash Point:226.6°C
PSA：112.55000
Density:1.28g/cm³
LogP:0.21430

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-D-ribofuranosylamine

There total 1 articles about N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-D-ribofuranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51172-55-5
p-toluenesulfonate d'amino-1, O-isopropylidene-2',3', α,β-D-ribofurannose

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 157306-01-9
N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-β-D-ribofuranosylamine

: 157306-00-8
N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-α-D-ribofuranosylamine

Guidance literature:: With sodium methylate; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₃OH, 1 h, 2.) CH₃OH, overnight;
DOI:10.1016/0008-6215(94)80044-8

Reference yield: 50.0%

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 157306-00-8
N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-α-D-ribofuranosylamine

: 3,4,6-tri-O-benzoyl-α-D-glucose 1,2-

Guidance literature:: With molecular sieve; silver carbonate; In dichloromethane; for 3h;
DOI:10.1016/0008-6215(94)80044-8

Reference yield:

: 10257-28-0
D-Galactose

: 98-88-4
benzoyl chloride

: 157306-00-8
N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-α-D-ribofuranosylamine

: N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-5-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-α-D-ribofuranosylamine

: N-(2,2-diethoxycarbonylvinyl)-2,3-O-isopropylidene-5-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α-D-ribofuranosylamine

Guidance literature:: With pyridine; molecular sieve; hydrogen bromide; silver perchlorate; acetic acid; Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1016/0008-6215(94)80044-8