1,4-Benzenediamine, N-methyl-N'-phenyl-

Base Information

Chemical Name:1,4-Benzenediamine, N-methyl-N'-phenyl-
CAS No.:41286-42-4
Molecular Formula:C13H14N2
Molecular Weight:198.268
Hs Code.:
DSSTox Substance ID:DTXSID50396980
Nikkaji Number:J3.039.548D
Wikidata:Q82197966
Mol file:41286-42-4.mol

Synonyms:41286-42-4;1,4-Benzenediamine, N-methyl-N'-phenyl-;N1-Methyl-N-4-phenylbenzene-1,4-diamine;N1-METHYL-N4-PHENYLBENZENE-1,4-DIAMINE;1-N-methyl-4-N-phenylbenzene-1,4-diamine;Oprea1_138502;SCHEMBL784987;DTXSID50396980;N-Phenyl-N'-methylbenzene-1,4-diamine

Suppliers and Price of 1,4-Benzenediamine, N-methyl-N'-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,4-Benzenediamine, N-methyl-N'-phenyl-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:198.115698455
Heavy Atom Count:15
Complexity:167

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC1=CC=C(C=C1)NC2=CC=CC=C2

Technology Process of 1,4-Benzenediamine, N-methyl-N'-phenyl-

There total 4 articles about 1,4-Benzenediamine, N-methyl-N'-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1205-71-6
N-(4-chlorophenyl)aniline

: 74-89-5
methylamine

: 41286-42-4
N-[4-methylaminophenyl]-N-phenylamine

Guidance literature:: With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; sodium t-butanolate; In tetrahydrofuran; toluene; at 85 ℃; for 48h; chemoselective reaction; Inert atmosphere;
DOI:10.1021/jo202358p

Reference yield: 78.0%

: 75-52-5
nitromethane

: 2-(4-nitrophenyl)-1,3,2-dioxaborinane

: 98-80-6
phenylboronic acid

: 6911-87-1,211060-12-7
4-bromo-N-methylaniline

: 41286-42-4
N-[4-methylaminophenyl]-N-phenylamine

Guidance literature:: With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; diphenylsilane; at 120 ℃; for 12h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/jacs.0c08035

Reference yield:

: 24067-17-2
4-nitrophenylboronic acid

: 41286-42-4
N-[4-methylaminophenyl]-N-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 80 °C / Schlenk technique; Inert atmosphere

2: 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; diphenylsilane / 12 h / 120 °C / Schlenk technique; Inert atmosphere

With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; diphenylsilane; In toluene;
DOI:10.1021/jacs.0c08035