2,3-Naphthalenedicarboxylic acid, 1-(3,4-dimethoxyphenyl)-6,7-dimethoxy-, dimethyl ester

Base Information

Chemical Name:2,3-Naphthalenedicarboxylic acid, 1-(3,4-dimethoxyphenyl)-6,7-dimethoxy-, dimethyl ester
CAS No.:42298-60-2
Molecular Formula:C24H24O8
Molecular Weight:440.45
Hs Code.:
Mol file:42298-60-2.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Naphthalenedicarboxylic acid, 1-(3,4-dimethoxyphenyl)-6,7-dimethoxy-, dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2,3-Naphthalenedicarboxylic acid, 1-(3,4-dimethoxyphenyl)-6,7-dimethoxy-, dimethyl ester

There total 14 articles about 2,3-Naphthalenedicarboxylic acid, 1-(3,4-dimethoxyphenyl)-6,7-dimethoxy-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: C₁₆H₁₈O₆

: 866252-52-0
4,5-dimethoxy-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 42298-60-2
dimethyl 1-(3,4-dimethoxyphenyl)-6,7-dimethoxynaphthalene-2,3-dicarboxylate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; cesium fluoride; 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazolium chloride; In acetonitrile; at 60 ℃; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/ol3028658

Reference yield:

: dimethyl 6,7-dimethoxy-1-(((trifluoromethyl) sulfonyl)oxy)naphthalene-2,3-dicarboxylate

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: 42298-60-2
dimethyl 1-(3,4-dimethoxyphenyl)-6,7-dimethoxynaphthalene-2,3-dicarboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; In 1,4-dioxane; at 90 ℃; Inert atmosphere;
DOI:10.2174/1573406416666200610190417