Bis(2,4,6-trimethylphenyl)stannane

Base Information

• Chemical Name: Bis(2,4,6-trimethylphenyl)stannane
• CAS No.: 425613-21-4
• Molecular Formula: C18H24Sn
• Molecular Weight: 359.099
• DSSTox Substance ID: DTXSID20785488
• Wikidata: Q82751199

Synonyms:bis(2,4,6-trimethylphenyl)stannane;425613-21-4;DTXSID20785488

Chemical Property of Bis(2,4,6-trimethylphenyl)stannane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 358.074353
• Heavy Atom Count: 19
• Complexity: 235

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1)C)[Sn]C2=C(C=C(C=C2C)C)C)C

Technology Process of Bis(2,4,6-trimethylphenyl)stannane

There total 4 articles about Bis(2,4,6-trimethylphenyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

[(cyclopentadienyl)(pentamethylcyclopentadienyl)HfCl(Sn(H)(mesityl)2)] + hydrogen (1333-74-0) → (η5-C5H5)(η5-C5Me5)HfHCl + bis(2,4,6-trimethylphenyl)stannane (425613-21-4) + (SnH((CH3)3C6H2)2)2 (425613-27-0)

Guidance literature:

In benzene; 1 atm of H2, 2 days;

DOI:10.1021/ja017495s

Reference yield: 54.0%

lithium aluminium tetrahydride (16853-85-3) + dimesityltin dichloride (108343-63-1) → bis(2,4,6-trimethylphenyl)stannane (425613-21-4)

Guidance literature:

In diethyl ether; at 0 ℃; for 1h;

DOI:10.1002/ejic.201900180

Reference yield: 21.0%

Sn(2)H2((CH3)3C6H2)2 (425613-35-0) + (SnH((CH3)3C6H2)2)2 (425613-27-0) → bis(2,4,6-trimethylphenyl)stannane (425613-21-4) + (Sn((CH3)3C6H2)2)2H(2)H (425613-41-8) + Sn(2)HH((CH3)3C6H2)2

Guidance literature:

In benzene-d6; 11 days, C6D6, 1.2 equiv; (1)NMR spectra;

DOI:10.1021/ja017495s

upstream raw materials:

Sn⁽²⁾H₂((CH₃)3C₆H₂)2

(SnH((CH₃)3C₆H₂)2)2

hydrogen

lithium aluminium tetrahydride

Downstream raw materials:

(SnH((CH₃)3C₆H₂)2)2

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