5-BENZYL-2-HYDROXY-BENZOIC ACID

Base Information

• Chemical Name: 5-BENZYL-2-HYDROXY-BENZOIC ACID
• CAS No.: 4386-41-8
• Molecular Formula: C14H12O3
• Molecular Weight: 228.24300
• Hs Code.: 2918290000
• Mol file: 4386-41-8.mol

Synonyms:4-Oxy-diphenylmethan-carbonsaeure-(3);5-BENZYL-2-HYDROXY-BENZOIC ACID;5-Benzyl-2-hydroxy-benzoesaeure;5-Benzyl-salicylsaeure;

Chemical Property of 5-BENZYL-2-HYDROXY-BENZOIC ACID

Chemical Property:

• PSA: 57.53000
• LogP: 2.68120

Purity/Quality:

97% ^*data from raw suppliers

5-Benzyl-2-hydroxybenzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-BENZYL-2-HYDROXY-BENZOIC ACID

There total 10 articles about 5-BENZYL-2-HYDROXY-BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydroxy-5-(α-hydroxy-benzyl)-benzoic acid → 5-benzyl-2-hydroxy-benzoic acid (4386-41-8)

Guidance literature:

With ammonium hydroxide; aluminium amalgam;

Reference yield:

<4-hydroxy-3-(methoxycarbonyl)phenyl>phenylmethane (41876-46-4) → 5-benzyl-2-hydroxy-benzoic acid (4386-41-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1017/S0317167100001748

Reference yield:

5-bromosalicyclic acid (89-55-4) → 5-benzyl-2-hydroxy-benzoic acid (4386-41-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) t-BuLi / 1.) THF, pentane, -90 to -40 deg C, 2.a) 1 h, b) r.t., overnight

2: H₂ / Pd/C

With hydrogen; tert.-butyl lithium; palladium on activated charcoal;

DOI:10.1021/jo00067a048

upstream raw materials:

<4-hydroxy-3-(methoxycarbonyl)phenyl>phenylmethane

p-benzylphenol

carbon dioxide

5-bromosalicyclic acid

Downstream raw materials:

<4-hydroxy-3-(methoxycarbonyl)phenyl>phenylmethane

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