Copper, [(4-methoxyphenyl)ethynyl]-

Base Information

Chemical Name:Copper, [(4-methoxyphenyl)ethynyl]-
CAS No.:48121-13-7
Molecular Formula:C9H7CuO
Molecular Weight:194.7
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Copper, [(4-methoxyphenyl)ethynyl]-

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Technology Process of Copper, [(4-methoxyphenyl)ethynyl]-

There total 11 articles about Copper, [(4-methoxyphenyl)ethynyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8
copper

: 768-60-5
4-methoxyphenylacetylen

: 48121-13-7
copper(I) 4-methoxyphenylacetylenide

Guidance literature:: With Et₄N(CH₃C₆H₄SO₃); In acetonitrile; at 20 ℃; for 4h; Electrochemical reaction;
DOI:10.1039/c9ra06782e

Reference yield: 92.0%

: 768-60-5
4-methoxyphenylacetylen

: 48121-13-7
copper(I) 4-methoxyphenylacetylenide

Guidance literature:: With hydroxylamine hydrochloride; ammonia; copper(II) sulfate; In ethanol; water; for 0.0833333h;

Reference yield: 86.0%

: 7681-65-4
copper(l) iodide

: 768-60-5
4-methoxyphenylacetylen

: 48121-13-7
copper(I) 4-methoxyphenylacetylenide

Guidance literature:: With hydroxylamine hydrochloride; In ammonium hydroxide; ethanol; under N2 atm. using Schlenk techniques; soln. of CuI in satd. aq. NH3 stirred for 1 h; H2NOH*HCl added; mixt. added to soln. of 4-methoxyphenylacetylene in EtOH (preliminarily stirred for 1 h); mixt. stirred at 20°C for 10 h; ppt. filtered off; washed (H2O, EtOH, Et2O); dried in desiccator at 20°C (1 Torr) for 4 h;
DOI:10.1023/B:RUCB.0000030827.50273.da