ethylidenecyclobutane

Base Information

• Chemical Name: ethylidenecyclobutane
• CAS No.: 1528-21-8
• Molecular Formula: C6H10
• Molecular Weight: 82.1454
• Mol file: 1528-21-8.mol

Synonyms:Ethylidenecyclobutane

Chemical Property of ethylidenecyclobutane

Chemical Property:

• Vapor Pressure: 96.3mmHg at 25°C
• Boiling Point: 80°Cat760mmHg
• Flash Point: °C
• Density: 0.931g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethylidenecyclobutane

There total 9 articles about ethylidenecyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

cyclobutanone (1191-95-3) + ethylenetriphenylphosphorane (1754-88-7) → ethylidenecyclobutane (1528-21-8)

Guidance literature:

In dimethyl sulfoxide; for 0.5h; Ambient temperature;

DOI:10.1021/ja00125a010

Reference yield:

acetamide (60-35-5) + 1,1,1-tri(bromomethyl)propane (6974-30-7) → 2-ethyl-1-butene (760-21-4) + ethylcyclobutane (4806-61-5) + vinylcyclobutane (2597-49-1) + ethylidenecyclobutane (1528-21-8)

Guidance literature:

at 110 ℃; Produkt 5: 1-Methyl-1-aethyl-cyclopropan;

Reference yield:

1,1,1-tri(bromomethyl)propane (6974-30-7) → vinylcyclobutane (2597-49-1) + ethylidenecyclobutane (1528-21-8)

Guidance literature:

With sodium carbonate; sodium iodide; zinc; at 110 ℃; Reagens 4: Acetamid;

upstream raw materials:

1,1,1-tri(bromomethyl)propane

propene

methylidenecyclobutane

1,1,1-tri(hydroxymethyl)propane

Downstream raw materials:

1,1'-bi(cyclobutylidene)