1,1,2,2-Tetramethyl-1,2,3,6-tetrahydro-1,2-disiline

Base Information

• Chemical Name: 1,1,2,2-Tetramethyl-1,2,3,6-tetrahydro-1,2-disiline
• CAS No.: 51043-84-6
• Molecular Formula: C8H18Si2
• Molecular Weight: 170.402
• DSSTox Substance ID: DTXSID60508476
• Nikkaji Number: J1.756.476E
• Wikidata: Q82365429
• Mol file: 51043-84-6.mol

Synonyms:51043-84-6;1,1,2,2-Tetramethyl-1,2,3,6-tetrahydro-1,2-disiline;DTXSID60508476;1,1,2,2-tetramethyl-1,2-disilacyclohex-4-ene

Chemical Property of 1,1,2,2-Tetramethyl-1,2,3,6-tetrahydro-1,2-disiline

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 170.09470364
• Heavy Atom Count: 10
• Complexity: 139

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si]1(CC=CC[Si]1(C)C)C

Technology Process of 1,1,2,2-Tetramethyl-1,2,3,6-tetrahydro-1,2-disiline

There total 1 articles about 1,1,2,2-Tetramethyl-1,2,3,6-tetrahydro-1,2-disiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-diallyl-1,1,2,2-tetramethyl-1,2-disilane (18645-49-3) → ethene (74-85-1) + 1,1,2,2-tetramethyl-1,2-disilacyclohex-4-ene (51043-84-6)

Guidance literature:

With aluminum oxide; tetra-n-butyltin(IV); rhenium(VII) oxide; for 4h; Yield given. Yields of byproduct given;

DOI:10.1007/BF00963715

Reference yield: 16.0%

1,1,2,2-tetramethyl-1,2-disilacyclohex-4-ene (51043-84-6) → 1,1-Dimethylsilacyclopent-3-en (16054-12-9) + trimethylsilan (993-07-7) + 1,1-dimethyl-1,3-disilacyclobutanes (38512-90-2) + 1,3-dimethyl-1,3-disilacyclobutane (1628-01-9)

Guidance literature:

at 750 ℃; under 0.01 Torr; Further byproducts given;

DOI:10.1016/0022-328X(84)80162-X

Reference yield: 15.0%

trans,trans-1,4-Diphenyl-1,3-butadiene (886-65-7,538-81-8) + 1,1,2,2-tetramethyl-1,2-disilacyclohex-4-ene (51043-84-6) → buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) + 1,1,2,2-tetramethyl-3,6-diphenyl-1,2,3,6-tetrahydro-[1,2]disiline (38512-91-3)

Guidance literature:

at 550 ℃; under 0.01 Torr;

DOI:10.1016/0022-328X(84)80162-X

upstream raw materials:

1,2-diallyl-1,1,2,2-tetramethyl-1,2-disilane

Downstream raw materials:

2,2,3,3-tetramethyl-5,6,7,8-tetraphenyl-1,2,3,4-tetrahydro-benzo[d][1,2]disiline

1,1,2,2-tetramethyl-1,2-disilacyclohexane

buta-1,3-diene

1,1,2,2-tetramethyl-3,6-diphenyl-1,2,3,6-tetrahydro-[1,2]disiline

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