3-(4-Methoxyphenyl)-3,4-dihydro-2H-1,3-benzoxazine

Base Information

Chemical Name:3-(4-Methoxyphenyl)-3,4-dihydro-2H-1,3-benzoxazine
CAS No.:51892-02-5
Molecular Formula:C15H15NO2
Molecular Weight:241.29
Hs Code.:
DSSTox Substance ID:DTXSID20554934
Nikkaji Number:J485.780A
Wikidata:Q82436126
Mol file:51892-02-5.mol

Synonyms:51892-02-5;3-(4-methoxyphenyl)-2,4-dihydro-1,3-benzoxazine;3-(4-Methoxyphenyl)-3,4-dihydro-2H-1,3-benzoxazine;SCHEMBL12162760;DTXSID20554934;3-(4-methoxyphenyl)-3,4-dihydro-2h-benzo[e][1,3]oxazine

Suppliers and Price of 3-(4-Methoxyphenyl)-3,4-dihydro-2H-1,3-benzoxazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-(4-Methoxyphenyl)-3,4-dihydro-2H-1,3-benzoxazine

Chemical Property:

PSA：21.70000
LogP:3.11670
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:241.110278721
Heavy Atom Count:18
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N2CC3=CC=CC=C3OC2

Technology Process of 3-(4-Methoxyphenyl)-3,4-dihydro-2H-1,3-benzoxazine

There total 11 articles about 3-(4-Methoxyphenyl)-3,4-dihydro-2H-1,3-benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 52537-88-9
N-(2-hydroxybenzyl)-p-anisidine

: 51892-02-5
3-(4-methoxyphenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: In ethanol; for 5h; Heating;

Reference yield: 65.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 104-94-9
4-methoxy-aniline

: 108-95-2,27073-41-2
phenol

: 51892-02-5
3-(4-methoxyphenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: In toluene; for 7h; Reflux;
DOI:10.1039/c6ra04420d

Reference yield: 61.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 104-94-9
4-methoxy-aniline

: 98-80-6
phenylboronic acid

: 51892-02-5
3-(4-methoxyphenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: With tert.-butylhydroperoxide; potassium carbonate; In dichloromethane; water; at 80 ℃; for 8h; Solvent; Sealed tube;
DOI:10.1016/j.tetlet.2017.02.081