1-bromo-3-nitronaphthalene

Base Information

Chemical Name:1-bromo-3-nitronaphthalene
CAS No.:7499-65-2
Molecular Formula:C10H6 Br N O2
Molecular Weight:252.067
Hs Code.:
Mol file:7499-65-2.mol

Synonyms:NSC 407684

Suppliers and Price of 1-bromo-3-nitronaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 1-bromo-3-nitronaphthalene

Chemical Property:

Vapor Pressure:4.07E-05mmHg at 25°C
Melting Point:132.3°C
Refractive Index:1.6120 (estimate)
Boiling Point:362.3°Cat760mmHg
Flash Point:172.9°C
PSA：45.82000
Density:1.662g/cm³
LogP:4.03370

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-bromo-3-nitronaphthalene

There total 10 articles about 1-bromo-3-nitronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 90767-01-4
4-bromo-2-nitro-1-naphthylamine

: 7499-65-2
4-bromo-2-nitronaphthalene

Guidance literature:: 4-bromo-2-nitro-1-naphthylamine; With sulfuric acid; acetic acid; sodium nitrite; at 5 - 20 ℃; for 2h;

With hypophosphorous acid; copper(II) sulfate; In ethanol; at 65 ℃; for 1h;

Reference yield:

: 7499-73-2
N-(4-bromo-2-nitronaphthalen-1-yl)acetamide

: 7499-65-2
4-bromo-2-nitronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₂SO₄ / ethanol

2: (deamination)

With sulfuric acid; In ethanol;
DOI:10.1021/jo01067a044

Reference yield:

: 91394-66-0
1-(acetylamino)-4-bromonaphthalene

: 7499-65-2
4-bromo-2-nitronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: NO₂/HNO₃ / acetic acid

2: aq. H₂SO₄ / ethanol

3: (deamination)

With sulfuric acid; nitric acid; Nitrogen dioxide; In ethanol; acetic acid;
DOI:10.1021/jo01067a044