Stannolane, 1,1-diphenyl-

Base Information

Chemical Name:Stannolane, 1,1-diphenyl-
CAS No.:53561-93-6
Molecular Formula:C16H18Sn
Molecular Weight:329.029
Hs Code.:

Synonyms:

Suppliers and Price of Stannolane, 1,1-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Stannolane, 1,1-diphenyl-

Chemical Property:

Vapor Pressure:0mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Stannolane, 1,1-diphenyl-

There total 3 articles about Stannolane, 1,1-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5274-40-8
1,4-bis(triphenylstannyl)butane

: 53561-93-6
1,1-diphenylstannacyclopentane

: 595-90-4
tetraphenyltin(IV)

Guidance literature:: With zinc(II) chloride;

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 1135-99-5
diphenyltin(IV) dichloride

: 7439-95-4
magnesium

: 53561-93-6
1,1-diphenylstannacyclopentane

Guidance literature:: With HCl; In diethyl ether; addn. of 1,4-dibromobutane in dry ether to Mg turnings, slow addn. of diphenyl tin dichloride in dry ether (room temp.), refluxing (3 h), cooling, hydrolysis by pouring in ice-cold 1M HCl; decanting of organic layer, washing (10% KF soln.), decanting, drying (MgSO4), removing of solvent, distn. of residual oil (401-403 K, 13 Pa), solidification (refrigerator), recrystn. (pentane, 2 times); elem. anal.;
DOI:10.1016/0021-9614(88)90220-0