2-Propene (dithioic) acid, 3-hydroxy-3-phenyl-

Base Information

Chemical Name:2-Propene (dithioic) acid, 3-hydroxy-3-phenyl-
CAS No.:41467-11-2
Molecular Formula:C9H8 O S2
Molecular Weight:0
Hs Code.:2930909090
Mol file:41467-11-2.mol

Synonyms:NSC 304620

Suppliers and Price of 2-Propene (dithioic) acid, 3-hydroxy-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 2-Propene (dithioic) acid, 3-hydroxy-3-phenyl-

Chemical Property:

Vapor Pressure:0.00128mmHg at 25°C
Boiling Point:298.3°C at 760 mmHg
Flash Point:134.2°C
PSA：91.12000
Density:1.234g/cm³
LogP:2.84270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Propene (dithioic) acid, 3-hydroxy-3-phenyl-

There total 2 articles about 2-Propene (dithioic) acid, 3-hydroxy-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-15-0,12122-00-8
carbon disulfide

: 98-86-2
acetophenone

: 41467-11-2
3-hydroxy-3-phenyl-2-propenedithioic acid

Guidance literature:: With potassium tert-butylate; In di-isopropyl ether; at 20 - 30 ℃; Inert atmosphere;
DOI:10.1139/cjc-2012-0325

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 100-52-7
benzaldehyde

: 41467-11-2
3-hydroxy-3-phenyl-2-propenedithioic acid

Guidance literature:: benzaldehyde; With sodium hydride; In tetrahydrofuran;

carbon disulfide; In tetrahydrofuran;
DOI:10.2147/IDR.S328132

Reference yield: 70.0%

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 41467-11-2
3-hydroxy-3-phenyl-2-propenedithioic acid

: 126723-87-3
cis-(PPh₃)2Pt{2-benzoyl-1,1-ethenedithiolate}

Guidance literature:: With NaOAc; In dichloromethane; byproducts: NaCl; dropwise addn. of the cinnamic acid in CH2Cl2 to a suspn. of cis-(Ph3P)2PtCl2 and NaOAc in CH2Cl2 under N2, stirring of the deep red soln. (room temp., 12 h), evapn. to dryness, digesting with CH2Cl2, filtration through celite, addn. of hexane; careful redn. of vol., pptn., washing (hexane, 2-3 times), drying (high vac.); elem. anal.;