Acetic acid, (methylamino)oxo-, methyl ester

Base Information

• Chemical Name: Acetic acid, (methylamino)oxo-, methyl ester
• CAS No.: 54154-11-9
• Molecular Formula: C4H7NO3
• Molecular Weight: 117.104

Synonyms:methyl-oxalamic acid methyl ester;N-Methyloxamsaeure-methylester;Methyl-oxalamidsaeure-methylester;N-methyloxansaeuremethylester;Oxalsaeuremethylester-N-methylamid;N-Methyl-oxamidsaeure-methylester;

Chemical Property of Acetic acid, (methylamino)oxo-, methyl ester

Chemical Property:

• Melting Point: 78 °C(Solv: ethyl ether (60-29-7); ligroine (8032-32-4))
• PSA: 55.40000
• Density: 1.126±0.06 g/cm3(Predicted)
• LogP: -0.70370

Purity/Quality:

Methyl(methylcarbamoyl)formate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetic acid, (methylamino)oxo-, methyl ester

There total 11 articles about Acetic acid, (methylamino)oxo-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-(methylamino)-2-oxoacetic acid (29262-58-6) → methyl 2-(methylamino)-2-oxoacetate (54154-11-9)

Guidance literature:

With diazomethane; In methanol; diethyl ether; for 0.333333h;

DOI:10.1016/j.ejps.2005.11.010

Reference yield: 80.0%

4-(dimethylamino)-5,5-dimethyl-1-(N-methyloxamoyl)-2H,5H-imidazol-2-on (87179-07-5) → methyl 2-(methylamino)-2-oxoacetate (54154-11-9) + 5-(Dimethylamino)-3,4-dihydro-4,4-dimethyl-2H-imidazol-2-on (73766-15-1)

Guidance literature:

In methanol;

DOI:10.1002/hlca.19830660514

Reference yield: 79.0%

methanol (67-56-1) + 4-(dimethylamino)-5,5-dimethyl-1-(N-methyloxamoyl)-2H,5H-imidazol-2-on (87179-07-5) → methyl 2-(methylamino)-2-oxoacetate (54154-11-9) + 5-(Dimethylamino)-3,4-dihydro-4,4-dimethyl-2H-imidazol-2-on (73766-15-1)

Guidance literature:

for 48h; Ambient temperature; reflux, 2 h;

DOI:10.1002/hlca.19930760617

upstream raw materials:

Dimethyl oxalate

methylamine

methanol

4-(dimethylamino)-5,5-dimethyl-1-(N-methyloxamoyl)-2H,5H-imidazol-2-on

Downstream raw materials:

1-phenyl-3-methyl-2,4-(1H,3H)quinazolinedione

2-(phenylamino)benzoic acid

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