13-Oxa-2,8,11-triazapentadecanoic acid, 7-carboxy-8-[(9H-fluoren-9-ylmethoxy)carbonyl]-14,14-dimethyl-12-oxo-, 1-[(2-chlorophenyl)methyl] ester, (7R)-

Base Information

Chemical Name:13-Oxa-2,8,11-triazapentadecanoic acid, 7-carboxy-8-[(9H-fluoren-9-ylmethoxy)carbonyl]-14,14-dimethyl-12-oxo-, 1-[(2-chlorophenyl)methyl] ester, (7R)-
CAS No.:548490-53-5
Molecular Formula:C36H42ClN3O8
Molecular Weight:680.198
Hs Code.:

13-Oxa-2,8,11-triazapentadecanoic acid,
7-carboxy-8-[(9H-fluoren-9-ylmethoxy)carbonyl]-14,14-dimethyl-12-oxo-,
1-[(2-chlorophenyl)methyl] ester, (7R)-

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Chemical Property of 13-Oxa-2,8,11-triazapentadecanoic acid, 7-carboxy-8-[(9H-fluoren-9-ylmethoxy)carbonyl]-14,14-dimethyl-12-oxo-, 1-[(2-chlorophenyl)methyl] ester, (7R)-

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Technology Process of 13-Oxa-2,8,11-triazapentadecanoic acid, 7-carboxy-8-[(9H-fluoren-9-ylmethoxy)carbonyl]-14,14-dimethyl-12-oxo-, 1-[(2-chlorophenyl)methyl] ester, (7R)-

There total 2 articles about 13-Oxa-2,8,11-triazapentadecanoic acid, 7-carboxy-8-[(9H-fluoren-9-ylmethoxy)carbonyl]-14,14-dimethyl-12-oxo-, 1-[(2-chlorophenyl)methyl] ester, (7R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 548490-52-4
2-[(2-tert-butoxycarbonylamino-ethyl)-(9H-fluoren-9-ylmethoxycarbonyl)-amino]-6-(2-chloro-benzyloxycarbonylamino)-hexanoic acid allyl ester

: 548490-53-5
2-[(2-tert-butoxycarbonylamino-ethyl)-(9H-fluoren-9-ylmethoxycarbonyl)-amino]-6-(2-chloro-benzyloxycarbonylamino)-hexanoic acid

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;
DOI:10.1002/ejoc.200390148

Reference yield: 60.0%

: 548490-54-6
2-(2-tert-butoxycarbonylamino-ethylamino)-6-(2-chloro-benzyloxycarbonylamino)-hexanoic acid

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 548490-53-5
2-[(2-tert-butoxycarbonylamino-ethyl)-(9H-fluoren-9-ylmethoxycarbonyl)-amino]-6-(2-chloro-benzyloxycarbonylamino)-hexanoic acid

Guidance literature:: With bis-(trimethylsilyl)acetamide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/ejoc.200390148