2-Tert-butyl-5-methylpyridine

Base Information

Chemical Name:2-Tert-butyl-5-methylpyridine
CAS No.:56029-43-7
Molecular Formula:C10H15N
Molecular Weight:149.23300
Hs Code.:
DSSTox Substance ID:DTXSID20497837
Nikkaji Number:J2.949.603J
Wikidata:Q82347607
Mol file:56029-43-7.mol

Synonyms:2-TERT-BUTYL-5-METHYLPYRIDINE;56029-43-7;2-(tert-Butyl)-5-methylpyridine;SCHEMBL146646;DTXSID20497837;MVPXJVKKNFNIQH-UHFFFAOYSA-N;AKOS015892021;FT-0720917

Suppliers and Price of 2-Tert-butyl-5-methylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Tert-butyl-5-methylpyridine

Chemical Property:

PSA：12.89000
LogP:2.68750
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:149.120449483
Heavy Atom Count:11
Complexity:123

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CN=C(C=C1)C(C)(C)C

Technology Process of 2-Tert-butyl-5-methylpyridine

There total 9 articles about 2-Tert-butyl-5-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-99-6
3-Methylpyridine

: 38442-51-2
tert-butylmercury chloride

: 56029-43-7
2-(tert-butyl)-5-methylpyridine

Guidance literature:: at 40 ℃; for 20h; Irradiation;
DOI:10.1021/jo00218a041

Reference yield: 54.0%

: 1003-73-2
3-picoline-N-oxide

: 3282-30-2
pivaloyl chloride

: 56029-43-7
2-(tert-butyl)-5-methylpyridine

Guidance literature:: With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; In acetonitrile; at 24 ℃; for 12h; Irradiation;
DOI:10.1021/acs.orglett.8b01250

Reference yield:

: 108-99-6
3-Methylpyridine

: 56029-43-7
2-(tert-butyl)-5-methylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 24 °C

1.2: 4 h

2.1: (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate / acetonitrile / 12 h / 24 °C / Irradiation

With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1021/acs.orglett.8b01250