Benzamide, N-[[[3-[[5-oxido-4-(phenylsulfonyl)-1,2,5-oxadiazol-3-yl]oxy]propyl]amino] [[3-[1-(triphenylmethyl)-1H-imidazol-4-yl]propyl]amino]methylene]-

Base Information

Chemical Name:Benzamide, N-[[[3-[[5-oxido-4-(phenylsulfonyl)-1,2,5-oxadiazol-3-yl]oxy]propyl]amino] [[3-[1-(triphenylmethyl)-1H-imidazol-4-yl]propyl]amino]methylene]-
CAS No.:565446-69-7
Molecular Formula:C44H41N7O6S
Molecular Weight:795.919
Hs Code.:

Benzamide,
N-[[[3-[[5-oxido-4-(phenylsulfonyl)-1,2,5-oxadiazol-3-yl]oxy]propyl]amino]
[[3-[1-(triphenylmethyl)-1H-imidazol-4-yl]propyl]amino]methylene]-

Synonyms:

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Chemical Property of Benzamide, N-[[[3-[[5-oxido-4-(phenylsulfonyl)-1,2,5-oxadiazol-3-yl]oxy]propyl]amino] [[3-[1-(triphenylmethyl)-1H-imidazol-4-yl]propyl]amino]methylene]-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzamide, N-[[[3-[[5-oxido-4-(phenylsulfonyl)-1,2,5-oxadiazol-3-yl]oxy]propyl]amino] [[3-[1-(triphenylmethyl)-1H-imidazol-4-yl]propyl]amino]methylene]-

There total 19 articles about Benzamide, N-[[[3-[[5-oxido-4-(phenylsulfonyl)-1,2,5-oxadiazol-3-yl]oxy]propyl]amino] [[3-[1-(triphenylmethyl)-1H-imidazol-4-yl]propyl]amino]methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 66074-00-8
3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

: 565446-54-0
N-benzoyl-N'-(3-hydroxypropyl)-N-{3-[(1-triphenylmethyl)-imidazol-4-yl]propyl}guanidine

: 565446-69-7
N-[3-(4-benzenesulfonyl-5-oxy-furazan-3-yloxy)-propyl]-N'-benzoyl-N''-[3-(1-trityl-1H-imidazol-4-yl)-propyl]-guanidine

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 20 - 25 ℃; for 1h;
DOI:10.1016/S0968-0896(02)00651-X

Reference yield:

: 96797-15-8
N-trityl-4⁽⁵⁾-iodoimidazole

: 565446-69-7
N-[3-(4-benzenesulfonyl-5-oxy-furazan-3-yloxy)-propyl]-N'-benzoyl-N''-[3-(1-trityl-1H-imidazol-4-yl)-propyl]-guanidine

Guidance literature:: Multi-step reaction with 7 steps

1.1: EtMgBr / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

1.2: 82 percent / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

2.1: NaNH₂ / tetrahydrofuran / Heating

3.1: H₂ / Pd/C / tetrahydrofuran

4.1: LiAlH₄; AlCl₃ / diethyl ether; tetrahydrofuran / 1 h / 20 °C

5.1: 86 percent / CH₂Cl₂ / 0.5 h / 20 °C

6.1: 61 percent / tetrahydrofuran / 0.67 h / Heating

7.1: 88 percent / aq. NaOH / tetrahydrofuran / 1 h / 20 - 25 °C

With sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; ethylmagnesium bromide; hydrogen; sodium amide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/S0968-0896(02)00651-X

Reference yield:

: 154312-79-5
1-trityl-4-(2-cyanoethyl)imidazole

: 565446-69-7
N-[3-(4-benzenesulfonyl-5-oxy-furazan-3-yloxy)-propyl]-N'-benzoyl-N''-[3-(1-trityl-1H-imidazol-4-yl)-propyl]-guanidine

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Pd/C / tetrahydrofuran

2: LiAlH₄; AlCl₃ / diethyl ether; tetrahydrofuran / 1 h / 20 °C

3: 86 percent / CH₂Cl₂ / 0.5 h / 20 °C

4: 61 percent / tetrahydrofuran / 0.67 h / Heating

5: 88 percent / aq. NaOH / tetrahydrofuran / 1 h / 20 - 25 °C

With sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/S0968-0896(02)00651-X