1,4,6,9-Tetrathiaspiro[4.4]nonane

Base Information

• Chemical Name: 1,4,6,9-Tetrathiaspiro[4.4]nonane
• CAS No.: 13145-46-5
• Molecular Formula: C5H8 S4
• Molecular Weight: 196.383
• DSSTox Substance ID: DTXSID10157054
• Nikkaji Number: J102.247D
• Wikidata: Q83025174
• Mol file: 13145-46-5.mol

Synonyms:1,4,6,9-Tetrathiaspiro[4.4]nonane;13145-46-5;1,4,6,9-Tetrathiaspiro(4.4)nonane;Orthocarbonic acid, tetrathio-, cyclic diethylene ester;SCHEMBL1402814;DTXSID10157054;OIXFQRVSKVVDFW-UHFFFAOYSA-N

Chemical Property of 1,4,6,9-Tetrathiaspiro[4.4]nonane

Chemical Property:

• Vapor Pressure: 0.00165mmHg at 25°C
• Boiling Point: 303.6°Cat760mmHg
• Flash Point: 225.2°C
• PSA: 101.20000
• Density: 1.5g/cm³
• LogP: 2.55770
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 195.95088495
• Heavy Atom Count: 9
• Complexity: 84

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CSC2(S1)SCCS2

Technology Process of 1,4,6,9-Tetrathiaspiro[4.4]nonane

There total 2 articles about 1,4,6,9-Tetrathiaspiro[4.4]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-<1,2-ethanediylbis(thio)>bis-1,3-dithiolane (33145-02-7) + ethylene dibromide (106-93-4) → 1,3-dithiolane-2-thione (822-38-8) + 1,4,6,9-tetrathiaspiro<4.4>nonane (13145-46-5)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -5-(-10) grad C, 30 min, nitrogen, 2.) THF, 1 h at -5-(-10) grad C then 24 h at room temp.;

DOI:10.1016/S0040-4039(01)92515-8

Reference yield:

→ 1,4,6,9-tetrathiaspiro<4.4>nonane (13145-46-5)

Guidance literature:

aus 2-Cyanimino-1,3-thiolan;

DOI:10.1021/jo01283a046

Reference yield: 36.0%

1,4,6,9-tetrathiaspiro<4.4>nonane (13145-46-5) + 2-carboxybenzene diazonium chloride (4661-46-5) → 1,3-dithiolane-2-thione (822-38-8) + 2-thioxo-1,3-benzodithiole (934-36-1) + phenylthioethylene (1822-73-7)

Guidance literature:

With methyloxirane; In 1,2-dichloro-ethane; for 1h; Heating;

upstream raw materials:

2,2'-<1,2-ethanediylbis(thio)>bis-1,3-dithiolane

ethylene dibromide

Downstream raw materials:

1,3-dithiolane-2-thione

2-thioxo-1,3-benzodithiole

phenylthioethylene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 13145-46-5 1,4,6,9-Tetrathiaspiro[4.4]nonane

Send

Send

Metric Ton KG G Pound L ML

Send

Send