4-Chloro-n,n-dipropylbenzamide

Base Information

Chemical Name:4-Chloro-n,n-dipropylbenzamide
CAS No.:2447-87-2
Molecular Formula:C₁₃H₁₈ClNO
Molecular Weight:239.745
Hs Code.:
NSC Number:6038
DSSTox Substance ID:DTXSID80947363
Nikkaji Number:J788.159B
Wikidata:Q82925151
Mol file:2447-87-2.mol

Synonyms:4-chloro-n,n-dipropylbenzamide;2447-87-2;4-Chloro-N,N-di-n-propylbenzamide;NSC 6038;NSC6038;CBMicro_011566;N,N-Dipropyl-4-chlorobenzamide;DTXSID80947363;BCP32797;CAA44787;NSC-6038;SMSF0005611;MFCD01011335;AKOS003283602;CB14741;BIM-0011618.P001;CS-0103178;SR-01000206342;SR-01000206342-1

Suppliers and Price of 4-Chloro-n,n-dipropylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

DC Chemicals
NSC6038 >98%
100 mg
$ 350.00

DC Chemicals
NSC6038 >98%
1 g
$ 1400.00

DC Chemicals
NSC6038 >98%
250 mg
$ 700.00

American Custom Chemicals Corporation
4-CHLORO-N,N-DI-N-PROPYLBENZAMIDE 95.00%
5MG
$ 497.32

Total 9 raw suppliers

Chemical Property of 4-Chloro-n,n-dipropylbenzamide

Chemical Property:

Vapor Pressure:2.36E-05mmHg at 25°C
Boiling Point:359.6°Cat760mmHg
PKA:-1.42±0.70(Predicted)
Flash Point:171.3°C
PSA：20.31000
Density:1.076g/cm³
LogP:3.60220
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:239.1076919
Heavy Atom Count:16
Complexity:206

Purity/Quality:

98% ^*data from raw suppliers

NSC6038 >98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCN(CCC)C(=O)C1=CC=C(C=C1)Cl

Technology Process of 4-Chloro-n,n-dipropylbenzamide

There total 4 articles about 4-Chloro-n,n-dipropylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874-59-9
4-chlorobenzoyl bromide

: 142-84-7
di-n-propylamine

: 2447-87-2
4-chloro-N,N-dipropylbenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2018.08.026

Reference yield:

: 74-11-3
para-chlorobenzoic acid

: 2447-87-2
4-chloro-N,N-dipropylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / Ambient temperature

2: 1.) CF₃SO₃Me, 2.) N-methylmorpholine / 1.) ClCH₂CH₂Cl, RT, 5 min, 2.) ClCH₂CH₂Cl, 82 deg C, 1.5 h

With 4-methyl-morpholine; methyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1055/s-1996-4399

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 2447-87-2
4-chloro-N,N-dipropylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: dibromoisocyanuric acid / dichloromethane / 20 °C

2: triethylamine / dichloromethane / 0.17 h / 20 °C

With dibromoisocyanuric acid; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2018.08.026