3-phenyl-

Base Information

• Chemical Name: 3-phenyl-
• CAS No.: 5155-87-3
• Molecular Formula: C10H10O2
• Molecular Weight: 162.188
• Mol file: 5155-87-3.mol

Synonyms:2-Phenyl-propen-(2)-carbonsaeure-(1);3-phenyl-3-butenoic acid;β-Phenyl-Δβ-butensaeure;3-Phenyl-but-3-ensaeure;3-Phenyl-but-3-enoic acid;3-phenbylbut-3-enoic acid;

Chemical Property of 3-phenyl-

Chemical Property:

• Melting Point: 48 - 49 °C (ethyl acetate)
• Boiling Point: 302.9±11.0 °C(Predicted)
• PSA: 37.30000
• Density: 1.108±0.06 g/cm3(Predicted)
• LogP: 2.17450

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-phenyl-

There total 27 articles about 3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-Carboxy-2-hydroxy-4-phenyl-pent-4-en-saeure (96472-76-3) → 3-phenylbut-3-enoic acid (5155-87-3)

Guidance literature:

With pyridine; sodium periodate; for 1h;

DOI:10.1021/ja00527a064

Reference yield: 77.0%

phenylzinc(II) bromide (38111-44-3) + 3-iodo-3-butenoic acid (157104-38-6) → 3-phenylbut-3-enoic acid (5155-87-3)

Guidance literature:

dichloro bis(acetonitrile) palladium(II); In diethyl ether; N,N-dimethyl-formamide; at 25 ℃; for 12h;

DOI:10.1021/jo0007579

Reference yield: 73.0%

carbon dioxide (124-38-9,18923-20-1) + [3-(benzenesulfonyl)prop-1-en-2-yl]benzene (74866-37-8) → 3-phenylbut-3-enoic acid (5155-87-3)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 30 ℃; for 6h; Electrolysis;

DOI:10.1021/acs.joc.1c01261

upstream raw materials:

α-<2-Hydroxy-2.2-dicyano-ethyl>-styrol

carbon dioxide

(3-phenoxyprop-1-en-2-yl)benzene

4-methyleneoxetan-2-one

Downstream raw materials:

2-Phenyl-1-buten-4-ol-(4,4-d⁽²⁾)

3-methylenebenzenepropanoic acid methyl ester

3-phenylbutyric acid

(R)-3-phenylbutyric acid