1-(2,2-DiMethoxy-ethyl)-2-isocyano-benzene

Base Information

Chemical Name:1-(2,2-DiMethoxy-ethyl)-2-isocyano-benzene
CAS No.:592479-02-2
Molecular Formula:C11H13NO2
Molecular Weight:191.23
Hs Code.:
Mol file:592479-02-2.mol

Synonyms:o-(2,2-dimethoxyethyl)phenyl isocyanide;2-(2,2-dimethoxyethyl)phenyl isocyanide;1-(2,2-dimethoxyethyl)-2-isocyanobenzene;1-isocyano-2-(2,2-dimethoxyethyl)benzene;2-(2,2-dimethoxyethyl)phenyl isonitrile;

Suppliers and Price of 1-(2,2-DiMethoxy-ethyl)-2-isocyano-benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-(2,2-Dimethoxy-ethyl)-2-isocyano-benzene
50mg
$ 265.00

Chemcia Scientific
1-(2,2-Dimethoxy-ethyl)-2-isocyano-benzene 90%
2.5 G
$ 1995.00

Chemcia Scientific
1-(2,2-Dimethoxy-ethyl)-2-isocyano-benzene 90%
1 G
$ 995.00

Chemcia Scientific
1-(2,2-Dimethoxy-ethyl)-2-isocyano-benzene 90%
0.5 G
$ 665.00

Total 3 raw suppliers

Chemical Property of 1-(2,2-DiMethoxy-ethyl)-2-isocyano-benzene

Chemical Property:

PSA：18.46000
LogP:1.62950

Purity/Quality:

97% ^*data from raw suppliers

1-(2,2-Dimethoxy-ethyl)-2-isocyano-benzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(2,2-DiMethoxy-ethyl)-2-isocyano-benzene

There total 6 articles about 1-(2,2-DiMethoxy-ethyl)-2-isocyano-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 592478-96-1
N-[2-(2,2-dimethoxyethyl)phenyl]formamide

: 592479-02-2
2-(2-isocyanophenyl)acetaldehyde dimethyl acetal

Guidance literature:: With triethylamine; trichlorophosphate;
DOI:10.1016/S0040-4039(03)01040-2

Reference yield:

2-(2-nitrophenyl)acetaldehyde dimethyl acetal: 79844-33-0
2-(2-nitrophenyl)acetaldehyde dimethyl acetal

: 592479-02-2
2-(2-isocyanophenyl)acetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / H₂ / Pd/C / methanol / 760.05 Torr

2: 95 percent / KHMDS / tetrahydrofuran; toluene / 30 h / Heating

3: 96 percent / triethylamine; POCl₃ / CH₂Cl₂ / 2 h / 23 °C

With hydrogen; potassium hexamethylsilazane; triethylamine; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ol701446y

Reference yield:

: 32989-69-8
trans-2-nitro-β-pyrrolidinostyrene

: 592479-02-2
2-(2-isocyanophenyl)acetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 4 steps

1: chlorotrimethylsilane / 36 h / Heating

2: 93 percent / H₂ / Pd/C / methanol / 760.05 Torr

3: 95 percent / KHMDS / tetrahydrofuran; toluene / 30 h / Heating

4: 96 percent / triethylamine; POCl₃ / CH₂Cl₂ / 2 h / 23 °C

With chloro-trimethyl-silane; hydrogen; potassium hexamethylsilazane; triethylamine; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ol701446y