[1,1'-Biphenyl]-2,2'-dicarboxylic acid, 4,5,5',6,6'-pentamethoxy-4'-[2,3,4-trimethoxy-6-(methoxycarbonyl)phen oxy]-, dimethyl ester

Base Information

Chemical Name:[1,1'-Biphenyl]-2,2'-dicarboxylic acid, 4,5,5',6,6'-pentamethoxy-4'-[2,3,4-trimethoxy-6-(methoxycarbonyl)phen oxy]-, dimethyl ester
CAS No.:59252-29-8
Molecular Formula:C₃₂H₃₆O₁₅
Molecular Weight:660.629
Hs Code.:

Synonyms:trimethylocta-O-methylvalonate;(+/-)-5,6,4',5',6'-Pentamethoxy-4-(2,3,4-trimethoxy-6-methoxycarbonyl-phenoxy)-diphensaeure-dimethylester;(+/-)-5,6,4',5',6'-pentamethoxy-4-(2,3,4-trimethoxy-6-methoxycarbonyl-phenoxy)-diphenic acid dimethyl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1'-Biphenyl]-2,2'-dicarboxylic acid, 4,5,5',6,6'-pentamethoxy-4'-[2,3,4-trimethoxy-6-(methoxycarbonyl)phen oxy]-, dimethyl ester

Chemical Property:

PSA：161.97000
LogP:4.57450

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [1,1'-Biphenyl]-2,2'-dicarboxylic acid, 4,5,5',6,6'-pentamethoxy-4'-[2,3,4-trimethoxy-6-(methoxycarbonyl)phen oxy]-, dimethyl ester

There total 46 articles about [1,1'-Biphenyl]-2,2'-dicarboxylic acid, 4,5,5',6,6'-pentamethoxy-4'-[2,3,4-trimethoxy-6-(methoxycarbonyl)phen oxy]-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: glansrin D

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 4891-62-7,65995-60-0,71307-89-6
4,5,6,4',5',6'-Hexamethoxy-biphenyl-2,2'-dicarboxylic acid dimethyl ester

: 59252-29-8,118132-51-7,118964-21-9
trimethyl octa-O-methylvaloneate

Guidance literature:: diazomethane; glansrin D; In diethyl ether; ethanol; at 20 ℃;

With methanol; sodium methylate; at 20 ℃;
DOI:10.1021/jf062872b

Reference yield:

: 67-56-1
methanol

: 115520-82-6
nobotanin O

: 77-78-1
dimethyl sulfate

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 4891-62-7,65995-60-0,71307-89-6
dimethyl (S)-4,4',5,5',6,6'-hexamethoxydiphenoate

: 59252-29-8,118132-51-7,118964-21-9
(S)-6,6'-dimethyl-4-(6-methoxycarbonyl-2,3,4-trimethoxyphenoxy)-2,2',3,3',4'-pentamethoxy-1,1'-biphenyl dicarboxylate

Guidance literature:: nobotanin O; dimethyl sulfate; With potassium carbonate; In acetone; rt, overnight; reflux, 3 h;

methanol; With sodium hydroxide; at 20 ℃; for 6h;
DOI:10.1016/S0031-9422(99)00329-5