Pyrrolidine, 1-[[4-methoxy-3-(phenylmethoxy)phenyl]acetyl]-2-[2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-

Base Information

Chemical Name:Pyrrolidine, 1-[[4-methoxy-3-(phenylmethoxy)phenyl]acetyl]-2-[2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-
CAS No.:592529-09-4
Molecular Formula:C₃₁H₃₅NO₇
Molecular Weight:533.621
Hs Code.:

Synonyms:

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Chemical Property of Pyrrolidine, 1-[[4-methoxy-3-(phenylmethoxy)phenyl]acetyl]-2-[2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-

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Technology Process of Pyrrolidine, 1-[[4-methoxy-3-(phenylmethoxy)phenyl]acetyl]-2-[2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-

There total 3 articles about Pyrrolidine, 1-[[4-methoxy-3-(phenylmethoxy)phenyl]acetyl]-2-[2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54313-33-6
2-(3-(benzyloxy)-4-methoxyphenyl)acetyl chloride

: 592529-07-2
2-pyrrolidin-2-yl-1-(3,4,5-trimethoxy-phenyl)-ethanone

: 592529-09-4
2-{1-[2-(3-Benzyloxy-4-methoxy-phenyl)-acetyl]-pyrrolidin-2-yl}-1-(3,4,5-trimethoxy-phenyl)-ethanone

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/S0960-894X(03)00263-4

Reference yield:

: 139148-39-3
methyl 3-oxo-3-(3,4,5-trimethoxyphenyl)propanoate

: 592529-09-4
2-{1-[2-(3-Benzyloxy-4-methoxy-phenyl)-acetyl]-pyrrolidin-2-yl}-1-(3,4,5-trimethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: aq. KOH / 24 h / 20 °C

2: aq. phosphate buffer / 60 h / 20 °C / pH 7.0

3: Et₃N / CH₂Cl₂ / 20 °C

With potassium hydroxide; phosphate buffer; triethylamine; In dichloromethane;
DOI:10.1016/S0960-894X(03)00263-4

Reference yield:

: 114195-15-2
3-oxo-3-(3,4,5-trimethoxyphenyl)propionic acid

: 592529-09-4
2-{1-[2-(3-Benzyloxy-4-methoxy-phenyl)-acetyl]-pyrrolidin-2-yl}-1-(3,4,5-trimethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: aq. phosphate buffer / 60 h / 20 °C / pH 7.0

2: Et₃N / CH₂Cl₂ / 20 °C

With phosphate buffer; triethylamine; In dichloromethane;
DOI:10.1016/S0960-894X(03)00263-4