2-Methoxy-4-[(2-methylphenyl)iminomethyl]phenol

Base Information

• Chemical Name: 2-Methoxy-4-[(2-methylphenyl)iminomethyl]phenol
• CAS No.: 59675-15-9
• Molecular Formula: C15H15NO2
• Molecular Weight: 241.29
• DSSTox Substance ID: DTXSID50425249

Synonyms:ZINC00280715;59675-15-9;SCHEMBL3412010;DTXSID50425249;SR-01000209715;SR-01000209715-1

Chemical Property of 2-Methoxy-4-[(2-methylphenyl)iminomethyl]phenol

Chemical Property:

• XLogP3: 3.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 241.110278721
• Heavy Atom Count: 18
• Complexity: 280

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=CC=C1N=CC2=CC(=C(C=C2)O)OC

Technology Process of 2-Methoxy-4-[(2-methylphenyl)iminomethyl]phenol

There total 1 articles about 2-Methoxy-4-[(2-methylphenyl)iminomethyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

vanillin (121-33-5,8014-42-4) + o-toluidine (95-53-4) → 4-hydroxy-3-methoxybenzal-2-toluidine (59675-15-9)

Guidance literature:

In methanol; at 20 ℃;

Reference yield:

4-hydroxy-3-methoxybenzal-2-toluidine (59675-15-9) + copper(II) sulfate (7758-99-8) → Cu(C6H3(OH)(OCH3)(CHNC6H4CH3))2(H2O)2(2+)*SO4(2-) = [Cu(C6H3(OH)(OCH3)(CHNC6H4CH3))2(H2O)2]SO4 (90317-00-3)

Guidance literature:

In methanol; refluxed for 4-5 h; solvent destilled off, recrystd. from EtOH and petroleum ether repeatedly, elem. anal.;

Reference yield:

nickel(II) sulphate + 4-hydroxy-3-methoxybenzal-2-toluidine (59675-15-9) → Ni(C6H3(OH)(OCH3)(CHNC6H4CH3))2(H2O)4(2+)*SO4(2-) = [Ni(C6H3(OH)(OCH3)(CHNC6H4CH3))2(H2O)4]SO4 (90317-08-1)

Guidance literature:

In methanol; refluxed for 4-5 h; solvent destilled off, recrystd. from EtOH and petroleum ether repeatedly, elem. anal.;

upstream raw materials:

vanillin

o-toluidine

Downstream raw materials:

Cu(C₆H₃(OH)(OCH₃)(CHNC₆H₄CH₃))2(H₂O)2⁽²⁺⁾*SO₄^(2-) = [Cu(C₆H₃(OH)(OCH₃)(CHNC₆H₄CH₃))2(H₂O)2]SO₄

Ni(C₆H₃(OH)(OCH₃)(CHNC₆H₄CH₃))2(H₂O)4⁽²⁺⁾*SO₄^(2-) = [Ni(C₆H₃(OH)(OCH₃)(CHNC₆H₄CH₃))2(H₂O)4]SO₄

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