N-(4-Acetylphenyl)benzamide

Base Information

• Chemical Name: N-(4-Acetylphenyl)benzamide
• CAS No.: 5411-13-2
• Molecular Formula: C15H13 N O2
• Molecular Weight: 239.274
• Hs Code.: 2924299090
• Mol file: 5411-13-2.mol

Synonyms:Benzanilide,4'-acetyl- (6CI,7CI,8CI); 4-Benzamidoacetophenone; 4-Benzoylaminoacetophenone;4'-Acetylbenzanilide; N-(4-Acetylphenyl)benzamide;N-Benzoyl-4-aminoacetophenone; NSC 10921

Chemical Property of N-(4-Acetylphenyl)benzamide

Chemical Property:

• Vapor Pressure: 0.000211mmHg at 25°C
• Boiling Point: 326.8°Cat760mmHg
• Flash Point: 117.4°C
• PSA: 46.17000
• Density: 1.197g/cm³
• LogP: 3.21450

Purity/Quality:

99% ^*data from raw suppliers

N-(4-Acetylphenyl)benzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-Acetylphenyl)benzamide

There total 31 articles about N-(4-Acetylphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-phenyl benzoyl amide (93-98-1,5705-51-1) + acetic anhydride (108-24-7) → N-(4-acetylphenyl)benzamide (5411-13-2)

Guidance literature:

With lithium perchlorate; gallium(III) triflate; In nitromethane; at 50 ℃; for 24h;

DOI:10.1002/1615-4169(20010129)343:1<71::AID-ADSC71>3.0.CO;2-J

Reference yield: 98.0%

benzoyl chloride (98-88-4) + p-aminobenzophenone (99-92-3) → N-(4-acetylphenyl)benzamide (5411-13-2)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield: 98.0%

2-(4-acetylphenyl)-1H-isoindole-1,3(2H)-dione (40101-59-5) → N-(4-acetylphenyl)benzamide (5411-13-2)

Guidance literature:

With 1-methyl-pyrrolidin-2-one; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; water; potassium carbonate; at 150 ℃; for 6h; chemoselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.7b03278

upstream raw materials:

p-aminobenzophenone

carbon monoxide

(4-nitrophenyl)ethanone

benzene

Downstream raw materials:

N-{4-[2-(3-Hydroxy-2-oxo-2,3-dihydro-1H-indol-3-yl)-acetyl]-phenyl}-benzamide

benzoic acid-[4-(2-oxo-6-phenyl-1,2-dihydro-pyrimidin-4-yl)-anilide]

benzoic acid-[4-(5-phenyl-1⁽²⁾H-pyrazol-3-yl)-anilide]

4'-benzamido-2-bromoacetophenone

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