Pyridine, 2-[[[2,4,6-tris(1,1-dimethylethyl)phenyl]phosphinidene]methyl]-

Base Information

Chemical Name:Pyridine, 2-[[[2,4,6-tris(1,1-dimethylethyl)phenyl]phosphinidene]methyl]-
CAS No.:600179-11-1
Molecular Formula:C₂₄H₃₄NP
Molecular Weight:367.514
Hs Code.:

Synonyms:

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Chemical Property of Pyridine, 2-[[[2,4,6-tris(1,1-dimethylethyl)phenyl]phosphinidene]methyl]-

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Technology Process of Pyridine, 2-[[[2,4,6-tris(1,1-dimethylethyl)phenyl]phosphinidene]methyl]-

There total 1 articles about Pyridine, 2-[[[2,4,6-tris(1,1-dimethylethyl)phenyl]phosphinidene]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 83115-12-2
(2,4,6-tri-tert-butylphenyl)phosphine

: 144404-03-5,144404-05-7,600179-11-1
2-(2,4,6-Tri-tert-butyl-phenylphosphanylidenemethyl)-pyridine

Guidance literature:: With n-butyllithium; tert-butyldimethylsilyl chloride; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1016/S0040-4039(00)61192-9

Reference yield: 90.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 144404-03-5,600179-11-1,144404-05-7
(E)-((2-pyridyl)methylene)(2,4,6-tri-tert-butylphenyl)phosphine

: 186688-46-0
η(1),η(1)-[(E)-((2-pyridyl)methylene)(2,4,6-tri-tert-butylphenyl)phosphine]methylpalladium chloride

Guidance literature:: In dichloromethane; N2-atmosphere; stirring (room temp., 10 min); evapn. (reduced pressure), washing (ether / pentane), drying (vac.); elem. anal.;
DOI:10.1021/om960925g

Reference yield: 86.0%

: 153297-46-2
bis(2-phenylpyridine-C²,N)-bis(aquo)iridium(III) trifluoromethanesulfonate

: 144404-03-5,144404-05-7,600179-11-1
2-(2-pyridyl)phosphaethene

: 864358-25-8
Ir(2-pyridylphenyl)2(2-(2-pyridyl)phosphaethene)OTf

Guidance literature:: In dichloromethane; (under N2, Schlenk); ligand added to soln. of Ir-complex in CH2Cl2 with stirring, stirred at room temp. for 2 h; volatiles removed under reduced pressure, residue washed with Et2O, hexane at 0°C, dried under reduced pressure; elem. anal.;
DOI:10.1021/om700275s