5-BroMo-2-Methoxy-3-nitrobenzoic acid

Base Information

• Chemical Name: 5-BroMo-2-Methoxy-3-nitrobenzoic acid
• CAS No.: 60541-89-1
• Molecular Formula: C8H6BrNO5
• Molecular Weight: 276.043
• Hs Code.: 2918990090
• Mol file: 60541-89-1.mol

Synonyms:Benzoic acid,5-bromo-2-methoxy-3-nitro;5-bromo-2-methoxy-3-nitro-benzoic acid;5-Brom-2-methoxy-3-nitro-benzoesaeure;

Chemical Property of 5-BroMo-2-Methoxy-3-nitrobenzoic acid

Chemical Property:

• Melting Point: 147-148 °C(Solv: water (7732-18-5); methanol (67-56-1))
• Boiling Point: 408.7±45.0 °C(Predicted)
• PKA: 2.86±0.20(Predicted)
• PSA: 92.35000
• Density: 1.792±0.06 g/cm3(Predicted)
• LogP: 2.58730
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

5-Bromo-2-methoxy-3-nitrobenzoic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-BroMo-2-Methoxy-3-nitrobenzoic acid

There total 3 articles about 5-BroMo-2-Methoxy-3-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5-bromo-2-methoxybenzoic acid (2476-35-9) → 5-bromo-2-methoxy-3-nitro-benzoic acid (60541-89-1)

Guidance literature:

With sulfuric acid; nitric acid; at -10 - 0 ℃; for 0.166667h;

Reference yield:

5-bromosalicyclic acid (89-55-4) → 5-bromo-2-methoxy-3-nitro-benzoic acid (60541-89-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide

2: 75.3 percent / sulfuric acid; nitric acid / 0.5 h

With potassium hydroxide; sulfuric acid; nitric acid;

DOI:10.1021/jo062032w

Reference yield:

→ 5-bromo-2-methoxy-3-nitro-benzoic acid (60541-89-1)

Guidance literature:

5-Brom-2-methoxy-benzoesaeure, HNO3, H2SO4;

upstream raw materials:

5-bromo-2-methoxybenzoic acid

5-bromosalicyclic acid

Downstream raw materials:

5-bromo-2-methoxy-3-nitro-benzoic acid methyl ester

methyl 3-(4-fluorophenylsulfonamino)-2-methoxy-5-(4-morpholinoquinazolin-6-yl)benzoate

N,N-dimethyl-3-(4-fluorophenylsulfonamino)-2-methoxy-5-(4-morpholinoquinazolin-6-yl)benzamide

N-methyl-3-(4-fluorophenylsulfonamino)-2-methoxy-5-(4-morpholinoquinazolin-6-yl)benzamide

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