2-Diethoxyphosphoryl-2-phenylpropanal

Base Information

Chemical Name:2-Diethoxyphosphoryl-2-phenylpropanal
CAS No.:6172-08-3
Molecular Formula:C13H19O4P
Molecular Weight:270.265
Hs Code.:
DSSTox Substance ID:DTXSID20547568
Nikkaji Number:J673.427H

Synonyms:DTXSID20547568;2-diethoxyphosphoryl-2-phenylpropanal;6172-08-3;Diethyl (1-oxo-2-phenylpropan-2-yl)phosphonate;diethyl 1-methyl-2-oxo-1-phenylethylphosphonate

Suppliers and Price of 2-Diethoxyphosphoryl-2-phenylpropanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Diethoxyphosphoryl-2-phenylpropanal

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:270.10209608
Heavy Atom Count:18
Complexity:302

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(C(C)(C=O)C1=CC=CC=C1)OCC

Technology Process of 2-Diethoxyphosphoryl-2-phenylpropanal

There total 3 articles about 2-Diethoxyphosphoryl-2-phenylpropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6172-07-2
(3-methyl-3-phenyl-oxiranyl)-phosphonic acid diethyl ester

: 6172-08-3
α-Formyl-α-phenyl-aethyl-phosphonsaeurediaethylester

Guidance literature:: at 170 ℃; under 0.7 Torr;
DOI:10.1021/ja00960a049

Reference yield:

: 3167-63-3
diethyl chloromethylphosphonate

: 6172-08-3
α-Formyl-α-phenyl-aethyl-phosphonsaeurediaethylester

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran / -78 °C

2: BF₃*Et₂O / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) room temperature, 2 h

With n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 98-86-2
acetophenone

: 6172-08-3
α-Formyl-α-phenyl-aethyl-phosphonsaeurediaethylester

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran / -78 °C

2: BF₃*Et₂O / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) room temperature, 2 h

With n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;