Carbonothioic dihydrazide, bis(1-phenylethylidene)-

Base Information

Chemical Name:Carbonothioic dihydrazide, bis(1-phenylethylidene)-
CAS No.:5326-14-7
Molecular Formula:C₁₇H₁₈N₄S
Molecular Weight:310.423
Hs Code.:
NSC Number:268
DSSTox Substance ID:DTXSID20427735
Mol file:5326-14-7.mol

Synonyms:5326-14-7;Carbonothioic dihydrazide, bis(1-phenylethylidene)-;1-(1-phenylethylideneamino)-3-(1-phenylethylideneamino)thiourea;NSC268;DTXSID20427735;NSC-268;NCGC00332652-01;1,5-Bis(1-phenylethylidene)thiocarbonohydrazide;AB01325754-02;(2E)-N'-[(1E)-1-Phenylethylidene]-2-(1-phenylethylidene)hydrazine-1-carbothiohydrazide

Suppliers and Price of Carbonothioic dihydrazide, bis(1-phenylethylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Carbonothioic dihydrazide, bis(1-phenylethylidene)-

Chemical Property:

Boiling Point:444.1°Cat760mmHg
Flash Point:222.4°C
Density:1.12g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:310.12521776
Heavy Atom Count:22
Complexity:380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NNC(=S)NN=C(C)C1=CC=CC=C1)C2=CC=CC=C2
Isomeric SMILES:C/C(=N\NC(=S)N/N=C(/C1=CC=CC=C1)\C)/C2=CC=CC=C2

Technology Process of Carbonothioic dihydrazide, bis(1-phenylethylidene)-

There total 1 articles about Carbonothioic dihydrazide, bis(1-phenylethylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2231-57-4
Thiocarbohydrazide

: 98-86-2
acetophenone

: 5326-14-7
di(o-hydroxyacetophenone)thiocarbohydrazone

Guidance literature:: In ethanol; 1a) reflux, 3 h, 1b) glacial acetic acid, room temp., overnight;

Reference yield: 72.0%

: vanadyl(IV) sulphate pentahydrate

: 5326-14-7
diacetophenone thiocarbohydrazone

: [VO(C₆H₅C(CH₃)NNHCSNHNC(CH₃)C₆H₅)2H₂O]⁽²⁺⁾*SO₄^(2-)=[VO(C₆H₅C(CH₃)NNHCSNHNC(CH₃)C₆H₅)2H₂O]SO₄

Guidance literature:: With H₂O; In ethanol; water; mixing hot ethanolic soln. of ligand and hot water-ethanol soln. of metal salt; refluxing on water bath for about 2 h; concentrating soln. to half of original volume; cooling; filtration; washing with ethanol; drying in oven at 80°C; elem. anal.;
DOI:10.1016/S0277-5387(00)84562-3

Reference yield: 52.0%

: 5326-14-7
diacetophenone thiocarbohydrazone

: 10361-79-2
praseodymium(III) chloride

: 262291-38-3
Pr(C₁₇H₁₇N₄S)Cl₂

Guidance literature:: With potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide; byproducts: HCl; the ligand was added to a refluxing DMF-EtOH soln. (1:1) of PrCl3, followed by the addn. of an aq. ethanolic soln. of KOH, the mixt. was refluxed for 10 h, cooled to room temp.; Et2O was added, allowed to stand for 5-6 h, ppt. was filtered, washed with water and ether and recrystd. from DMF-Et2O-EtOH and dried in vac.; elem. anal.;
DOI:10.1080/00945710009351753