4-CHLORO-2-NITRO-1-(PHENYLTHIO)BENZENE

Base Information

• Chemical Name: 4-CHLORO-2-NITRO-1-(PHENYLTHIO)BENZENE
• CAS No.: 4548-56-5
• Molecular Formula: C12H8 Cl N O2 S
• Molecular Weight: 265.72
• Hs Code.: 2930909090
• Mol file: 4548-56-5.mol

Synonyms:Sulfide,4-chloro-2-nitrophenyl phenyl (6CI,7CI,8CI); 2-Nitro-4-chlorodiphenyl sulfide;4-Chloro-2-nitro-1-(phenylthio)benzene; NSC 658179

Chemical Property of 4-CHLORO-2-NITRO-1-(PHENYLTHIO)BENZENE

Chemical Property:

• Vapor Pressure: 1.99E-05mmHg at 25°C
• Melting Point: 82 °C
• Boiling Point: 373°Cat760mmHg
• Flash Point: 179.4°C
• PSA: 71.12000
• Density: 1.41g/cm³
• LogP: 4.92260

Purity/Quality:

99%, ^*data from raw suppliers

4-Chloro-2-nitro-1-(phenylthio)benzene 97% ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-2-NITRO-1-(PHENYLTHIO)BENZENE

There total 9 articles about 4-CHLORO-2-NITRO-1-(PHENYLTHIO)BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-fluoro-5-chloronitrobenzene (345-18-6) + thiophenol (108-98-5) → 4-chloro-2-nitrophenyl phenyl sulfide (4548-56-5)

Guidance literature:

With sodium hydroxide; In methanol; at 20 ℃; for 4h;

Reference yield: 92.0%

thiophenol (108-98-5) + 2,5-dichloronitrobenzene (89-61-2) → 4-chloro-2-nitrophenyl phenyl sulfide (4548-56-5)

Guidance literature:

With ammonium acetate; In ethanol; for 48h; Heating;

DOI:10.1016/S0968-0896(97)00070-9

Reference yield: 81.0%

4-chloro-2-nitro-benzoic acid (6280-88-2) + thiophenol (108-98-5) → 4-chloro-2-nitrophenyl phenyl sulfide (4548-56-5)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; oxygen; potassium carbonate; In dimethyl sulfoxide; at 140 ℃; for 24h; Molecular sieve;

DOI:10.1039/c6cc04486g

upstream raw materials:

thiophenol

2,5-dichloronitrobenzene

ethanol

sodium thiophenolate

Downstream raw materials:

5-chloro-2-phenylsulfanyl-aniline

4-chloro-2-nitrodiphenyl sulphone

2-chlorophenothiazine

4-chloro-2-(hydroxyamino)phenyl phenyl sulphide

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