3-Benzyloxy-1,2-diacetyl-1,2-propanediol

Base Information

• Chemical Name: 3-Benzyloxy-1,2-diacetyl-1,2-propanediol
• CAS No.: 13754-10-4
• Molecular Formula: C₁₄H₁₈O₅
• Molecular Weight: 266.294
• DSSTox Substance ID: DTXSID10864438
• Nikkaji Number: J50.753I
• Mol file: 13754-10-4.mol

Synonyms:3-Benzyloxy-1,2-diacetyl-1,2-propanediol;13754-10-4;1,2-Propanediol, 3-benzyloxy-1,2-diacetyl-;(2-acetyloxy-3-phenylmethoxypropyl) acetate;3-(Phenylmethoxy)-1,2-propanediol diacetate;DTXSID10864438;PZJWZGWBDMSONK-UHFFFAOYSA-N;3-(benzyloxy)propane-1,2-diyl diacetate;(+/-)-3-(benzyloxy)propane-1,2-diyl diacetate;2-(Acetyloxy)-1-[(benzyloxy)methyl]ethyl acetate #

Chemical Property of 3-Benzyloxy-1,2-diacetyl-1,2-propanediol

Chemical Property:

• Vapor Pressure: 2.15E-05mmHg at 25°C
• Boiling Point: 360.9°Cat760mmHg
• Flash Point: 157.3°C
• PSA: 0.00000
• Density: 1.133g/cm³
• LogP: 0.00000
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 9
• Exact Mass: 266.11542367
• Heavy Atom Count: 19
• Complexity: 284

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(=O)OCC(COCC1=CC=CC=C1)OC(=O)C

Technology Process of 3-Benzyloxy-1,2-diacetyl-1,2-propanediol

There total 47 articles about 3-Benzyloxy-1,2-diacetyl-1,2-propanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(R)-3-benzyloxy-1,2-propanediol (56552-80-8) + acetic anhydride (108-24-7) → (+)-(S)-1,2-di-O-acetyl-3-O-benzylpropane-1,2,3-triol (17325-86-9,13754-10-4)

Guidance literature:

With pyridine; for 12h; Ambient temperature;

DOI:10.1021/jo00073a030

Reference yield: 99.0%

(2S)-3-(benzyloxy)propane-1,2-diol (17325-85-8) + acetic anhydride (108-24-7) → (2R)-1,2-diacetoxy-3-(benzyloxy)propane (17325-87-0,13754-10-4)

Guidance literature:

With pyridine; for 12h; Ambient temperature;

DOI:10.1021/jo00073a030

Reference yield: 92.0%

(R)-3-benzyloxy-1,2-propanediol (56552-80-8) + acetyl chloride (75-36-5) → (+)-(S)-1,2-di-O-acetyl-3-O-benzylpropane-1,2,3-triol (17325-86-9,13754-10-4)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2.66667h;

DOI:10.5012/bkcs.2010.31.9.2689

upstream raw materials:

3-benzyloxypropan-1,2-diol

acetic anhydride

acetic acid

benzyl allyl ether

Downstream raw materials:

(2R)-1,2-diacetoxy-3-(benzyloxy)propane

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