Fluorene-1-carbonyl chloride

Base Information

• Chemical Name: Fluorene-1-carbonyl chloride
• CAS No.: 55341-64-5
• Molecular Formula: C14H9ClO
• Molecular Weight: 228.678
• Hs Code.: 2916399090
• NSC Number: 80181
• DSSTox Substance ID: DTXSID80292062
• Wikidata: Q82030202
• Mol file: 55341-64-5.mol

Synonyms:Fluorene-1-carbonyl chloride;9H-fluorene-1-carbonyl chloride;55341-64-5;NSC 80181;fluorenoyl chloride;Fluorencarbonsaurechlorid;fluorenecarboxylic acid chloride;SCHEMBL1327276;DTXSID80292062;NSC80181;NSC-80181;9H-fluorene-1-carboxylic acid chloride

Chemical Property of Fluorene-1-carbonyl chloride

Chemical Property:

• Vapor Pressure: 4.9E-06mmHg at 25°C
• Boiling Point: 381.9°Cat760mmHg
• Flash Point: 184.3°C
• PSA: 17.07000
• Density: 1.308g/cm³
• LogP: 3.63680
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 228.0341926
• Heavy Atom Count: 16
• Complexity: 289

Purity/Quality:

99% ^*data from raw suppliers

9H-FLUORENE-1-CARBONYLCHLORIDE 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C2=CC=CC=C2C3=C1C(=CC=C3)C(=O)Cl

Technology Process of Fluorene-1-carbonyl chloride

There total 4 articles about Fluorene-1-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.5%

9H-fluorene-1-carboxylic acid (6276-03-5) → 9H-fluorene-1-carboxyl chloride (55341-64-5)

Guidance literature:

With thionyl chloride; for 2h; Heating;

DOI:10.1021/jo00279a015

Reference yield: 76.0%

→ 9H-fluorene-1-carboxyl chloride (55341-64-5)

Guidance literature:

Reference yield:

oxalyl dichloride (79-37-8) + 9H-fluorene-1-carboxylic acid (6276-03-5) → 9H-fluorene-1-carboxyl chloride (55341-64-5)

Guidance literature:

In dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

9H-fluorene-1-carboxylic acid

9-oxo-9H-fluorene-1-carboxylic acid

oxalyl dichloride

Downstream raw materials:

fluoren-1-yl-phenyl ketone

fluorene-1-carbonyl azide

1-chloro-9H-fluorene

[1-Chloro-fluoren-(9E)-ylidenemethyl]-(4-chloro-phenyl)-amine