boronic acid, B-butyl-, dibutyl ester

Base Information

• Chemical Name: boronic acid, B-butyl-, dibutyl ester
• CAS No.: 3027-58-5
• Molecular Formula: C12H27 B O2
• Molecular Weight: 214.156
• Mol file: 3027-58-5.mol

Synonyms:1-Butaneboronicacid, dibutyl ester (6CI,7CI,8CI); Boronic acid, butyl-, dibutyl ester (9CI);Borane, dibutoxybutyl-; Dibutoxybutylboron; Dibutyl butylboronate

Chemical Property of boronic acid, B-butyl-, dibutyl ester

Chemical Property:

• Vapor Pressure: 0.262mmHg at 25°C
• Boiling Point: 211.64°C at 760 mmHg
• Flash Point: 81.797°C
• PSA: 18.46000
• Density: 0.82g/cm³
• LogP: 3.90810

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of boronic acid, B-butyl-, dibutyl ester

There total 3 articles about boronic acid, B-butyl-, dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tributyl borane (122-56-5) + oxygen (80937-33-3) → boric acid tributyl ester (688-74-4) + dibutoxybutylboron (3027-58-5)

Guidance literature:

With 2,6,10,15,19,23-hexamethyltetracosane; at 30 ℃; Inert atmosphere;

DOI:10.1007/s11164-012-0512-2

Reference yield:

tributyl borane (122-56-5) + oxygen (80937-33-3) → boric acid tributyl ester (688-74-4) + dibutoxybutylboron (3027-58-5) + tri-n-butylboroxine (7359-98-0) + C12H27BO3 (108749-85-5)

Guidance literature:

With 2,4-dimethylpentane; at 30 ℃; Inert atmosphere;

DOI:10.1007/s11164-012-0512-2

Reference yield:

1,2-di-n-butyl-1,2-bis(dimethylamino) diborane (4887-12-1) + butan-1-ol (71-36-3) → dibutoxybutylboron (3027-58-5) + dimethyl amine (124-40-3)

Guidance literature:

byproducts: H2; 60-80°C;

upstream raw materials:

1,2-di-n-butyl-1,2-bis(dimethylamino) diborane

butan-1-ol

tributyl borane

oxygen

Downstream raw materials:

n-C₄H₉B(NHC₆H₅)2

Refernces