2,3,4-Trichloroanisole

Base Information

Chemical Name:2,3,4-Trichloroanisole
CAS No.:54135-80-7
Molecular Formula:C7H5 Cl3 O
Molecular Weight:211.475
Hs Code.:
European Community (EC) Number:258-990-7
UNII:FT5R63843S
DSSTox Substance ID:DTXSID10202477
Nikkaji Number:J209.016C
Wikidata:Q83075752
Mol file:54135-80-7.mol

Synonyms:2,3,4-Trichloroanisole;54135-80-7;2,3,4-Trichloroanisol;1,2,3-TRICHLORO-4-METHOXYBENZENE;Benzene, 1,2,3-trichloro-4-methoxy-;FT5R63843S;EINECS 258-990-7;SCHEMBL53547;UNII-FT5R63843S;DTXSID10202477;1,2,3-Trichloro-4-methoxy-benzene;MFCD00000541;1,2,3-Trichloro-4-methoxybenzene #;AKOS024319556;1,2,3-tris(chloranyl)-4-methoxy-benzene;CS-0453417;FT-0640224;A829984;2,3,4-Trichloroanisole 10 microg/mL in Isooctane;2,3,4-Trichloroanisole, PESTANAL(R), analytical standard

Suppliers and Price of 2,3,4-Trichloroanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,3,4-Trichloroanisole
500mg
$ 695.00

Sigma-Aldrich
2,3,4-Trichloroanisole PESTANAL?, analytical standard
100 mg
$ 42.00

Sigma-Aldrich
2,3,4-Trichloroanisole PESTANAL
100mg-r
$ 40.70

Medical Isotopes, Inc.
2,3,4-Trichloroanisole
25 ml
$ 650.00

American Custom Chemicals Corporation
2,3,4-TRICHLOROANISOLE 95.00%
1G
$ 750.00

Alichem
2,3,4-Trichloroanisole
1g
$ 1564.50

Alichem
2,3,4-Trichloroanisole
500mg
$ 831.30

Alichem
2,3,4-Trichloroanisole
250mg
$ 489.60

AHH
2,3,4-Trichloroanisol 98%
5g
$ 290.00

Total 13 raw suppliers

Chemical Property of 2,3,4-Trichloroanisole

Chemical Property:

Vapor Pressure:0.0186mmHg at 25°C
Melting Point:70°C
Refractive Index:1.5510 (estimate)
Boiling Point:261.6°C at 760 mmHg
Flash Point:104.7°C
PSA：9.23000
Density:1.416g/cm³
LogP:3.65540
Water Solubility.:10.8mg/L(25 oC)
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:209.940598
Heavy Atom Count:11
Complexity:131

Purity/Quality:

98%min ^*data from raw suppliers

2,3,4-Trichloroanisole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39-24/25-22

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)Cl)Cl)Cl
Uses 2,3,4-Trichloroanisole, is an intermediate for the synthesis of some methoxy-polychlorobiphenyl, and 2,3,4,7,8-Pentachlorodibenzofuran (P237975), used as standards for analytical, toxic, and biological studies.

Technology Process of 2,3,4-Trichloroanisole

There total 6 articles about 2,3,4-Trichloroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 634-66-2
1,2,3,4,-tetrachlorobenzene

: 124-41-4
sodium methylate

: 50375-10-5
1,2,4-trichloro-3-methoxybenzene

: 54135-80-7
1,2,3-trichloro-4-methoxybenzene

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; at 120 ℃; for 1h;
DOI:10.1016/S0040-4020(01)97647-1

Reference yield: 4.0%

: 634-66-2
1,2,3,4,-tetrachlorobenzene

: 124-41-4
sodium methylate

: 74-88-4
methyl iodide

: 50375-10-5
1,2,4-trichloro-3-methoxybenzene

: 54135-80-7
1,2,3-trichloro-4-methoxybenzene

: 86607-59-2
2,4-Dichloro-1,3-dimethoxybenzene

: 90283-02-6
3,6-dichlorocatechol dimethyl ether

: 90283-00-4
3,4-dichloro-1,2-dimethoxybenzene

Guidance literature:: 1,2,3,4,-tetrachlorobenzene; sodium methylate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 120 ℃; for 3h; Inert atmosphere;

methyl iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.3762/bjoc.9.311