5,6-Bis(4-methoxyphenyl)-2,3-dihydro-1,4-dioxine

Base Information

Chemical Name:5,6-Bis(4-methoxyphenyl)-2,3-dihydro-1,4-dioxine
CAS No.:65564-60-5
Molecular Formula:C18H18O4
Molecular Weight:298.339
Hs Code.:
DSSTox Substance ID:DTXSID80356355
Wikidata:Q82135641

Synonyms:5,6-bis(4-methoxyphenyl)-2,3-dihydro-1,4-dioxine;65564-60-5;AB-131/42301497;DTXSID80356355

Suppliers and Price of 5,6-Bis(4-methoxyphenyl)-2,3-dihydro-1,4-dioxine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 5,6-Bis(4-methoxyphenyl)-2,3-dihydro-1,4-dioxine

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:298.12050905
Heavy Atom Count:22
Complexity:341

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=C(OCCO2)C3=CC=C(C=C3)OC

Technology Process of 5,6-Bis(4-methoxyphenyl)-2,3-dihydro-1,4-dioxine

There total 2 articles about 5,6-Bis(4-methoxyphenyl)-2,3-dihydro-1,4-dioxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.4%

: 119-52-8
4,4'-dimethoxybenzoin

: 107-21-1
ethylene glycol

: 65564-60-5
5,6-bis-(4-methoxy-phenyl)-2,3-dihydro-[1,4]dioxine

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 80 ℃; for 24h;
DOI:10.1080/00397919808003073

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 65564-60-5
5,6-bis-(4-methoxy-phenyl)-2,3-dihydro-[1,4]dioxine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent

2: 65.4 percent / p-toluenesulfonic acid / benzene / 24 h / 80 °C

With toluene-4-sulfonic acid; In benzene;
DOI:10.1080/00397919808003073