4-bromophenyl 4-nitrobenzoate

Base Information

• Chemical Name: 4-bromophenyl 4-nitrobenzoate
• CAS No.: 36718-65-7
• Molecular Formula: C13H8 Br N O4
• Molecular Weight: 322.1109
• Mol file: 36718-65-7.mol

Synonyms:Phenol,4-bromo-, 4-nitrobenzoate (9CI); 4-Bromophenyl 4-nitrobenzoate; 4-Nitrobenzoicacid 4-bromophenyl ester; NSC 6893; p-Bromophenyl p-nitrobenzoate

Chemical Property of 4-bromophenyl 4-nitrobenzoate

Chemical Property:

• Vapor Pressure: 1.95E-08mmHg at 25°C
• Boiling Point: 454.2°Cat760mmHg
• Flash Point: 228.5°C
• Density: 1.603g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-bromophenyl 4-nitrobenzoate

There total 5 articles about 4-bromophenyl 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-bromo-phenol (106-41-2) + 4-nitrobenzaldehdye (555-16-8) → 4-bromophenyl 4-nitrobenzoate (36718-65-7)

Guidance literature:

With sodium cyanide; copper(l) iodide; sodium hydroxide; In neat (no solvent); at 120 ℃; for 18h;

DOI:10.1002/aoc.3766

Reference yield: 35.0%

p-nitrobenzene iodide (636-98-6) + 4-bromo-phenol (106-41-2) + carbon monoxide (201230-82-2) → 4-bromophenyl 4-nitrobenzoate (36718-65-7)

Guidance literature:

With sodium hydroxide; palladium diacetate; In N,N-dimethyl-formamide; at 60 ℃; for 2h; under 760 Torr;

Reference yield:

4-bromo-phenol (106-41-2) + 4-nitro-benzoyl chloride (122-04-3) → 4-bromophenyl 4-nitrobenzoate (36718-65-7)

Guidance literature:

upstream raw materials:

phenyl 4-nitrobenzoate

4-bromo-phenol

4-nitro-benzoyl chloride

p-nitrobenzene iodide

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