Propiophenone, 3',4'-dimethoxy-2-hydroxy-2-methyl-

Base Information

Chemical Name:Propiophenone, 3',4'-dimethoxy-2-hydroxy-2-methyl-
CAS No.:67466-08-4
Molecular Formula:C₁₂H₁₆O₄
Molecular Weight:224.257
Hs Code.:
DSSTox Substance ID:DTXSID50217823
Wikidata:Q83094502

Synonyms:BRN 2616520;Propiophenone, 3',4'-dimethoxy-2-hydroxy-2-methyl-;3',4'-Dimethoxy-2-hydroxy-2-methylpropiophenone;67466-08-4;SCHEMBL7637437;DTXSID50217823;LS-125167;1-Propanone, 1-(3,4-dimethoxyphenyl)-2-hydroxy-2-methyl-

Suppliers and Price of Propiophenone, 3',4'-dimethoxy-2-hydroxy-2-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Propiophenone, 3',4'-dimethoxy-2-hydroxy-2-methyl-

Chemical Property:

Vapor Pressure:2.28E-05mmHg at 25°C
Boiling Point:345.8°Cat760mmHg
Flash Point:128.8°C
Density:1.123g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:224.10485899
Heavy Atom Count:16
Complexity:249

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C(=O)C1=CC(=C(C=C1)OC)OC)O

Technology Process of Propiophenone, 3',4'-dimethoxy-2-hydroxy-2-methyl-

There total 3 articles about Propiophenone, 3',4'-dimethoxy-2-hydroxy-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: 5041-27-0
1-isocyanatocyclohex-1-ene

: 663192-23-2
2-(3,4-dimethoxy-phenyl)-2-methoxy-5,5-dimethyl-2,5-dihydro-[1,3,4]oxadiazole

: 67466-08-4
2-Hydroxy-3',4'-dimethoxy-2-methyl-propiophenon

: 23263-21-0
methyl cyclohex-1-enylcarbamate

: 1,2-dimethoxy-4-[methoxy-(1-methoxy-1-methyl-ethoxy)-methyl]-benzene

Guidance literature:: 1-isocyanatocyclohex-1-ene; 2-(3,4-dimethoxy-phenyl)-2-methoxy-5,5-dimethyl-2,5-dihydro-[1,3,4]oxadiazole; In benzene; Heating;

methanol;

Reference yield:

: 14046-55-0
isobutyryl-3,4-dimethoxybenzene

: 67466-08-4
2-Hydroxy-3',4'-dimethoxy-2-methyl-propiophenon

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂, HBr / acetic acid

2: (i) NaOMe, MeOH, (ii) aq. H₂SO₄

With hydrogen bromide; bromine; In acetic acid;
DOI:10.1021/jm00332a013