2-oxo-1,2-diphenylethyl acetate

Base Information

• Chemical Name: 2-oxo-1,2-diphenylethyl acetate
• CAS No.: 62398-10-1
• Molecular Formula: C₁₆H₁₄O₃
• Molecular Weight: 254.285

Synonyms:

Chemical Property of 2-oxo-1,2-diphenylethyl acetate

Chemical Property:

• Vapor Pressure: 5.91E-06mmHg at 25°C
• Boiling Point: 379.3°Cat760mmHg
• Flash Point: 167.2°C
• PSA: 43.37000
• Density: 1.161g/cm³
• LogP: 3.17370

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-oxo-1,2-diphenylethyl acetate

There total 59 articles about 2-oxo-1,2-diphenylethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) + acetic acid (64-19-7,77671-22-8) → 2-acetoxy-2-phenylacetophenone (62398-10-1,84275-45-6,84275-46-7,574-06-1)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; at 20 ℃; for 1h;

Reference yield: 97.0%

2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) + acetyl chloride (75-36-5) → 2-acetoxy-2-phenylacetophenone (62398-10-1,84275-45-6,84275-46-7,574-06-1)

Guidance literature:

zirconium(IV) oxychloride; at 20 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2004.10.164

Reference yield: 88.0%

2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) → 2-acetoxy-2-phenylacetophenone (62398-10-1,84275-45-6,84275-46-7,574-06-1)

Guidance literature:

With sulfuric acid; acetic anhydride; In dichloromethane; water;

upstream raw materials:

phenyl benzyl ketone

benzoin monomethyl ether

acetic anhydride

2-hydroxy-2-phenylacetophenone

Downstream raw materials:

2-methyl-4,5-diphenyloxazole

2-methyl-4,5-diphenyl-1H-imidazole

1,1,2,2-tetraphenyl-ethanol

(E)-O,O'-diacetyl-1,2-diphenylethen-1,2-diol

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