4-(Dimethoxymethyl)-2,6-dimethoxyphenol

Base Information

• Chemical Name: 4-(Dimethoxymethyl)-2,6-dimethoxyphenol
• CAS No.: 66460-63-7
• Molecular Formula: C11H16O5
• Molecular Weight: 228.245
• DSSTox Substance ID: DTXSID00596539
• Wikidata: Q82491822

Synonyms:4-(Dimethoxymethyl)-2,6-dimethoxyphenol;66460-63-7;syringaldehyde dimethyl acetal;SCHEMBL6717421;DTXSID00596539

Chemical Property of 4-(Dimethoxymethyl)-2,6-dimethoxyphenol

Chemical Property:

• XLogP3: 1.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 228.09977361
• Heavy Atom Count: 16
• Complexity: 181

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC(=CC(=C1O)OC)C(OC)OC

Technology Process of 4-(Dimethoxymethyl)-2,6-dimethoxyphenol

There total 2 articles about 4-(Dimethoxymethyl)-2,6-dimethoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5-Bromovanilline dimethyl acetal (90875-24-4) + sodium methylate (124-41-4) → 4-Hydroxy-3,5-dimethoxy-benzaldehyd-dimethylacetal (66460-63-7)

Guidance literature:

With ethyl acetate; copper(I) bromide; In methanol; for 2h; Heating;

DOI:10.1016/S0040-4039(00)77477-6

Reference yield:

syringic aldehyde (134-96-3) + trimethyl orthoformate (149-73-5) → 4-Hydroxy-3,5-dimethoxy-benzaldehyd-dimethylacetal (66460-63-7)

Guidance literature:

With toluene-4-sulfonic acid;

DOI:10.1021/jm9508806 DOI:10.1016/S0968-0896(97)00113-2

Reference yield: 92.0%

1.3-propanedithiol (109-80-8) + 4-Hydroxy-3,5-dimethoxy-benzaldehyd-dimethylacetal (66460-63-7) → 2-(3,5-Dimethoxy-4-hydroxyphenyl)-1,3-dithiane

Guidance literature:

With Kaolinitic clay; In tetrachloromethane; for 4h; Heating;

DOI:10.1039/a706475f

upstream raw materials:

5-Bromovanilline dimethyl acetal

sodium methylate

syringic aldehyde

trimethyl orthoformate

Downstream raw materials:

(3aR,4R,10R)-10-(4-Hydroxy-3,5-dimethoxy-phenyl)-4-methoxy-3a,4,9,10-tetrahydro-3H-2-oxa-9,10a-diaza-cyclopenta[b]fluoren-1-one

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 66460-63-7 Phenol, 4-(dimethoxymethyl)-2,6-dimethoxy-

Send

Send

Metric Ton KG G Pound L ML

Send

Send