3-(2-Methoxyphenyl)-2-methylprop-2-enoic acid

Base Information

• Chemical Name: 3-(2-Methoxyphenyl)-2-methylprop-2-enoic acid
• CAS No.: 3368-15-8
• Molecular Formula: C11H12O3
• Molecular Weight: 192.214
• European Community (EC) Number: 654-006-9
• NSC Number: 408423
• DSSTox Substance ID: DTXSID30419722
• Nikkaji Number: J2.617.644A
• Wikidata: Q76306127

Synonyms:3368-15-8;849831-38-5;(E)-3-(2-Methoxyphenyl)-2-methylacrylic acid;2-Propenoic acid, 3-(2-methoxyphenyl)-2-methyl-;3-(2-methoxyphenyl)-2-methylprop-2-enoic acid;NSC408423;starbld0018802;DTXSID30419722;alpha-Methyl-2-methoxycinnamic acid;AKOS006273187;Cinnamic acid, O-methoxy-alpha-methyl-;NSC-408423;Cinnamic acid, 2-methoxy-.alpha.-methyl-;(2E)-3-(2-methoxyphenyl)-2-methyl-2-propenoic acid;(E)-3-(2-methoxyphenyl)-2-methyl-prop-2-enoic acid

Chemical Property of 3-(2-Methoxyphenyl)-2-methylprop-2-enoic acid

Chemical Property:

• Vapor Pressure: 7.02E-05mmHg at 25°C
• Boiling Point: 329.7°Cat760mmHg
• Flash Point: 128.2°C
• Density: 1.162g/cm³
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 192.078644241
• Heavy Atom Count: 14
• Complexity: 233

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=CC1=CC=CC=C1OC)C(=O)O
• Isomeric SMILES: C/C(=C\C1=CC=CC=C1OC)/C(=O)O

Technology Process of 3-(2-Methoxyphenyl)-2-methylprop-2-enoic acid

There total 8 articles about 3-(2-Methoxyphenyl)-2-methylprop-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-(2-methoxyphenyl)-2-methylacrylic acid (3368-15-8)

Guidance literature:

With ethanol; alkaline aqueous sodium hypochlorite;

DOI:10.1021/ja01269a065

Reference yield:

methyl-propanedioic acid (516-05-2) + ortho-anisaldehyde (135-02-4) → 3-(2-methoxyphenyl)-2-methylacrylic acid (3368-15-8)

Guidance literature:

With piperidine; pyridine;

DOI:10.1021/ja01551a048

Reference yield:

propionic acid anhydride (123-62-6) + ortho-anisaldehyde (135-02-4) → 3-(2-methoxyphenyl)-2-methylacrylic acid (3368-15-8)

Guidance literature:

With sodium proprionate; at 165 ℃; im geschlossenen Rohr;

upstream raw materials:

3-(2-methoxyphenyl)-2-methylacrylic acid methyl ester

2-methoxy-phenylamine

propionic acid anhydride

ortho-anisaldehyde

Downstream raw materials:

1-(2-methoxyphenyl)propan-2-one

3-(2-methoxy-phenyl)-2-methyl-propionic acid amide

2-(2-Amino-propyl)-phenol

(d,l)-2-methoxyamphetamine

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