Technology Process of Zirconium, tetrakis(2,4-pentanedionato-kappaO,kappaO')-, (SA-8-11''11''1'1'''1'1''')-
There total 20 articles about Zirconium, tetrakis(2,4-pentanedionato-kappaO,kappaO')-, (SA-8-11''11''1'1'''1'1''')- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetylacetonate;
In
toluene;
byproducts: MePh; Ar atmosphere; 0. degree.C, 2 h (excess of C5H8O2);
DOI:10.1007/BF00995720
- Guidance literature:
-
With
(C4H9)4NBF4;
In
acetonitrile;
Electrolysis; reaction of Zr anode with 30% soln. of acetylacetone in CH3CN with added 0.1 M Bu4NBF4, Pt cathode; addn. of ether-acetone mixture;; pptn.; drying in vacuo; crystallization from CH3CN;;
- Guidance literature:
-
zirconium chloride-tetrahydrofuran; acetylacetone;
for 2h;
With
triethylamine;
for 2h;
Reflux;
DOI:10.1016/j.ica.2022.120864