2-Propenoic acid, 3-[3-methoxy-4-[(trimethylsilyl)oxy]phenyl]-, trimethylsilyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 3-[3-methoxy-4-[(trimethylsilyl)oxy]phenyl]-, trimethylsilyl ester
• CAS No.: 67460-51-9
• Molecular Formula: C₁₆H₂₆O₄Si₂
• Molecular Weight: 338.551
• DSSTox Substance ID: DTXSID301347072
• Nikkaji Number: J46.873H,J512.509J
• Wikidata: Q63395292

Synonyms:2-Propenoic acid, 3-[3-methoxy-4-[(trimethylsilyl)oxy]phenyl]-, trimethylsilyl ester;Trimethylsilyl 3-methoxy-4-(trimethylsilyloxy)cinnamate;3-Methoxy-4-(trimethylsilyl)oxycinnamic acid trimethylsilyl ester;Cinnamic acid, 3-methoxy-4-(trimethylsiloxy)-, trimethylsilyl ester;67460-51-9;Ferulic acid, TMS;Ferulic acid, di-TMS;Ferulic acid, bis-TMS;Ferulic acid, (2TMS);Ferulic acid, 2TMS derivative;Trimethylsilyl 3-(3-methoxy-4-[(trimethylsilyl)oxy]phenyl)-2-propenoate;UQBSUVIBJIXFQT-PKNBQFBNSA-N;DTXSID301347072;10517-09-6;Cinnamic acid, 4-hydroxy-3-methoxy, TMS;Cinnamic acid, 4-hydroxy-3-methoxy, bis-TMS;Q63395292;3-[3-Methoxy-4-(trimethylsilyloxy)phenyl]propenoic acid trimethylsilyl ester;Trimethylsilyl (2E)-3-[3-methoxy-4-[(trimethylsilyl)oxy]phenyl]-2-propenoate

Chemical Property of 2-Propenoic acid, 3-[3-methoxy-4-[(trimethylsilyl)oxy]phenyl]-, trimethylsilyl ester

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 338.13696238
• Heavy Atom Count: 22
• Complexity: 396

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=CC(=C1)C=CC(=O)O[Si](C)(C)C)O[Si](C)(C)C
• Isomeric SMILES: COC1=C(C=CC(=C1)/C=C/C(=O)O[Si](C)(C)C)O[Si](C)(C)C

Technology Process of 2-Propenoic acid, 3-[3-methoxy-4-[(trimethylsilyl)oxy]phenyl]-, trimethylsilyl ester

There total 2 articles about 2-Propenoic acid, 3-[3-methoxy-4-[(trimethylsilyl)oxy]phenyl]-, trimethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,O-bis-(trimethylsilyl)-acetamide (10416-59-8) + (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid (1135-24-6,537-98-4) → (E)-3-(4-trimethylsiloxy-3-methoxyphenyl)acrylic acid trimethylsilyl ester (67460-51-9)

Guidance literature:

at 50 - 70 ℃; for 1h;

Reference yield:

(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid (1135-24-6,537-98-4) + N,O-Bis(trimethylsilyl)trifluoroacetamide (25561-30-2) → (E)-3-(4-trimethylsiloxy-3-methoxyphenyl)acrylic acid trimethylsilyl ester (67460-51-9)

Guidance literature:

In pyridine; at 70 ℃; for 0.25h;

DOI:10.1021/jf9902494

upstream raw materials:

N,O-bis-(trimethylsilyl)-acetamide

(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

N,O-Bis(trimethylsilyl)trifluoroacetamide

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