(2-AMINO-4,5-DIMETHOXY-PHENYL)-(5-METHYL-FURAN-2-YL)-METHANONE

Base Information

Chemical Name:(2-AMINO-4,5-DIMETHOXY-PHENYL)-(5-METHYL-FURAN-2-YL)-METHANONE
CAS No.:676546-90-0
Molecular Formula:C14H15NO4
Molecular Weight:261.27300
Hs Code.:
Mol file:676546-90-0.mol

Synonyms:(2-Amino-4,5-dimethoxy-phenyl)-(5-methyl-furan-2-yl)-methanone;(2-amino-4,5-dimethoxyphenyl)(5-methyl-2-furyl)methanone;

Suppliers and Price of (2-AMINO-4,5-DIMETHOXY-PHENYL)-(5-METHYL-FURAN-2-YL)-METHANONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(2-Amino-4,5-dimethoxyphenyl)(5-methylfuran-2-yl)methanone 97%
1g
$ 583.00

Total 1 raw suppliers

Chemical Property of (2-AMINO-4,5-DIMETHOXY-PHENYL)-(5-METHYL-FURAN-2-YL)-METHANONE

Chemical Property:

Melting Point:120 °C (Petroleum ether)
PSA：74.69000
LogP:2.99960

Purity/Quality:: (2-Amino-4,5-dimethoxyphenyl)(5-methylfuran-2-yl)methanone 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2-AMINO-4,5-DIMETHOXY-PHENYL)-(5-METHYL-FURAN-2-YL)-METHANONE

There total 4 articles about (2-AMINO-4,5-DIMETHOXY-PHENYL)-(5-METHYL-FURAN-2-YL)-METHANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 676546-91-1
(4,5-dimethoxy-2-nitrophenyl)-(5-methyl-2-furyl)-methanone

: 676546-90-0
(2-amino-4,5-dimethoxyphenyl)-(5-methyl-2-furyl)methanone

Guidance literature:: With iron; acetic acid; In water; ethyl acetate; for 6h; Reflux;
DOI:10.1055/s-0030-1260118

Reference yield:

: 677299-77-3
(3,4-dimethoxy-phenyl)-(5-methyl-furan-2-yl)-methanone

: 676546-90-0
(2-amino-4,5-dimethoxyphenyl)-(5-methyl-2-furyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / HNO₃; AcOH / 0.5 h / 0 - 20 °C

2: 85 percent / Fe; AcOH / H₂O; ethyl acetate / 6 h / Heating

With nitric acid; iron; acetic acid; In water; ethyl acetate;
DOI:10.1016/j.tet.2006.10.056

Reference yield:

: 14003-11-3
5-methylfuran-2-carbonyl chloride

: 676546-90-0
(2-amino-4,5-dimethoxyphenyl)-(5-methyl-2-furyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / benzene / 2.5 h / 55 - 60 °C

2: 65 percent / HNO₃; AcOH / 0.5 h / 0 - 20 °C

3: 85 percent / Fe; AcOH / H₂O; ethyl acetate / 6 h / Heating

With aluminium trichloride; nitric acid; iron; acetic acid; In water; ethyl acetate; benzene; 1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2006.10.056