Benzeneacetaldehyde, a-methyl-a-2-propenyl-, (R)-

Base Information

Chemical Name:Benzeneacetaldehyde, a-methyl-a-2-propenyl-, (R)-
CAS No.:67679-06-5
Molecular Formula:C12H14O
Molecular Weight:174.243
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneacetaldehyde, a-methyl-a-2-propenyl-, (R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzeneacetaldehyde, a-methyl-a-2-propenyl-, (R)-

There total 33 articles about Benzeneacetaldehyde, a-methyl-a-2-propenyl-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 34713-70-7
2-Phenylpropanal

: 107-18-6
allyl alcohol

: 111464-55-2
(S)-(+)-2-methyl-2-phenyl-4-pentenylaldehyde

: 67679-06-5
(R)-(-)-2-methyl-2-phenyl-4-pentenylaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; (1R,2R)-1,2-diaminocyclohexane; 6-hydroxy-4,8-diisopropyl-1,11-dimethyldibenzo[d,f][1,3,2]dioxaphosphepine-6-oxide; In toluene; at 40 ℃; for 16h; Reagent/catalyst; Solvent; Temperature; Catalytic behavior; Schlenk technique; Molecular sieve;
DOI:10.1021/acs.joc.0c02385

Reference yield: 84.0%

: (R)-2-methyl-2-phenylpent-4-enenitrile

: 67679-06-5
(R)-(-)-2-methyl-2-phenyl-4-pentenylaldehyde

Guidance literature:: (R)-2-methyl-2-phenylpent-4-enenitrile; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -78 ℃; for 3h; Inert atmosphere;

With potassium tartrate sodium salt; In tetrahydrofuran; hexane; water; Inert atmosphere;
DOI:10.1021/jacs.5b02810

Reference yield: 76.0%

: 591-87-7
Allyl acetate

: 34713-70-7
2-Phenylpropanal

: 67679-06-5
(R)-(-)-2-methyl-2-phenyl-4-pentenylaldehyde

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; C₂₅H₂₆N₂O; acetic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In methanol; at 25 ℃; for 72h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/acscatal.1c03449