Acetic acid, [2-(3-chlorobenzoyl)-4-methylphenoxy]-, ethyl ester

Base Information

Chemical Name:Acetic acid, [2-(3-chlorobenzoyl)-4-methylphenoxy]-, ethyl ester
CAS No.:677707-45-8
Molecular Formula:C18H17ClO4
Molecular Weight:332.784
Hs Code.:
DSSTox Substance ID:DTXSID50466697
Wikidata:Q82293312

Synonyms:677707-45-8;Acetic acid, [2-(3-chlorobenzoyl)-4-methylphenoxy]-, ethyl ester;DTXSID50466697

Suppliers and Price of Acetic acid, [2-(3-chlorobenzoyl)-4-methylphenoxy]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Acetic acid, [2-(3-chlorobenzoyl)-4-methylphenoxy]-, ethyl ester

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:332.0815367
Heavy Atom Count:23
Complexity:412

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)COC1=C(C=C(C=C1)C)C(=O)C2=CC(=CC=C2)Cl

Technology Process of Acetic acid, [2-(3-chlorobenzoyl)-4-methylphenoxy]-, ethyl ester

There total 2 articles about Acetic acid, [2-(3-chlorobenzoyl)-4-methylphenoxy]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 6280-54-2
3'-chloro-2-hydroxy-5-methyl-benzophenone

: 105-39-5
chloroacetic acid ethyl ester

: 677707-45-8
ethyl [2-(3-chlorobenzoyl)-4-methylphenoxy]acetate

Guidance literature:: With Montmorillonite K₁₀ clay; for 0.133333h; microwave irradiation;
DOI:10.1002/hc.10210

Reference yield:

: 6280-49-5
4-methylphenyl 3-chlorobenzoate

: 677707-45-8
ethyl [2-(3-chlorobenzoyl)-4-methylphenoxy]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / aluminum chloride / nitrobenzene / 0.5 h / Heating

2: 80 percent / potassium carbonate / acetone / 8 h / Heating

With aluminium trichloride; potassium carbonate; In nitrobenzene; acetone; 1: Fries rearrangement;
DOI:10.1016/j.bioorg.2004.04.003