Glycine, N-[2-[[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino]ethyl]-N-[[4- [[(4-methoxyphenyl)diphenylmethyl]amino]-2-oxo-1(2H)-pyrimidinyl]acet yl]-

Base Information

Chemical Name:Glycine, N-[2-[[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino]ethyl]-N-[[4- [[(4-methoxyphenyl)diphenylmethyl]amino]-2-oxo-1(2H)-pyrimidinyl]acet yl]-
CAS No.:682752-98-3
Molecular Formula:C40H43N5O7
Molecular Weight:705.811
Hs Code.:

Glycine,
N-[2-[[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino]ethyl]-N-[[4-
[[(4-methoxyphenyl)diphenylmethyl]amino]-2-oxo-1(2H)-pyrimidinyl]acet
yl]-

Synonyms:

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Chemical Property of Glycine, N-[2-[[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino]ethyl]-N-[[4- [[(4-methoxyphenyl)diphenylmethyl]amino]-2-oxo-1(2H)-pyrimidinyl]acet yl]-

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Technology Process of Glycine, N-[2-[[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino]ethyl]-N-[[4- [[(4-methoxyphenyl)diphenylmethyl]amino]-2-oxo-1(2H)-pyrimidinyl]acet yl]-

There total 7 articles about Glycine, N-[2-[[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino]ethyl]-N-[[4- [[(4-methoxyphenyl)diphenylmethyl]amino]-2-oxo-1(2H)-pyrimidinyl]acet yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 864776-35-2
methyl N-{2-[N'⁴-(4-methoxytrityl)-cytosin-1-yl]-acetyl}-N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)ethylamino]ethyl}glycinate

: 682752-98-3
N-{2-[N'⁴-(4-methoxytrityl)-cytosin-1-yl]-acetyl}-N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)ethylamino]ethyl}glycine

Guidance literature:: With caesium carbonate; In methanol; for 1.5h;
DOI:10.1016/j.tet.2005.06.003

Reference yield:

: 94142-97-9
2-(1-hydroxyethylidene)-5,5-dimethylcyclohexane-1,3-dione

: 682752-98-3
N-{2-[N'⁴-(4-methoxytrityl)-cytosin-1-yl]-acetyl}-N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)ethylamino]ethyl}glycine

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / N,N-diisopropyl-N-ethylamine / CH₂Cl₂; methanol / 16 h / 20 °C

2: bromo-tris-pyrrolidino-phosphonium hexafluorophosphate; N,N-diisopropyl-N-ethyl / dimethylformamide / 25 °C

3: 45 percent / aq. Cs₂CO₃ / methanol / 1.5 h

With N,N-diisopropyl-N-ethyl; caesium carbonate; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.06.003

Reference yield:

: 861857-04-7
methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

: 682752-98-3
N-{2-[N'⁴-(4-methoxytrityl)-cytosin-1-yl]-acetyl}-N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)ethylamino]ethyl}glycine

Guidance literature:: Multi-step reaction with 2 steps

1: bromo-tris-pyrrolidino-phosphonium hexafluorophosphate; N,N-diisopropyl-N-ethyl / dimethylformamide / 25 °C

2: 45 percent / aq. Cs₂CO₃ / methanol / 1.5 h

With N,N-diisopropyl-N-ethyl; caesium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.06.003