2-(2-Thenoyl)anisole

Base Information

• Chemical Name: 2-(2-Thenoyl)anisole
• CAS No.: 6933-34-2
• Molecular Formula: C12H10O2S
• Molecular Weight: 218.27200
• Mol file: 6933-34-2.mol

Synonyms:(2-Methoxy-phenyl)-[2]thienyl-keton;(2-methoxy-phenyl)-thiophen-2-yl-methanone;2-thienyl 2'-methoxyphenyl ketone;(2-methoxyphenyl)(2-thienyl) methanone;2-(o-Methoxybenzoyl-thiophen);(2-methoxy-phenyl)-[2]thienyl ketone;

Chemical Property of 2-(2-Thenoyl)anisole

Chemical Property:

• PSA: 54.54000
• LogP: 2.98770

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2-Thenoyl)anisole

There total 4 articles about 2-(2-Thenoyl)anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(2-hydroxyphenyl)(thiophen-2-yl)methanone (20409-64-7) + dimethyl sulfate (77-78-1) → (2-methoxyphenyl)thiophen-2-ylmethanone (6933-34-2)

Guidance literature:

With sodium hydroxide; In ethanol; water; for 0.5h; Heating;

DOI:10.1002/ardp.19953280505

Reference yield: 68.0%

2-Iodothiophene (3437-95-4,149762-92-5) + carbon monoxide (201230-82-2) + 2-Methoxyphenylboronic acid (5720-06-9) → (2-methoxyphenyl)thiophen-2-ylmethanone (6933-34-2)

Guidance literature:

2-Iodothiophene; 2-Methoxyphenylboronic acid; With potassium carbonate; In toluene; for 0.166667h; Autoclave;

carbon monoxide; In toluene; at 100 ℃; for 10h; under 10343.2 Torr; Autoclave;

DOI:10.1055/s-0030-1258349

Reference yield:

thiophene (188290-36-0,8014-23-1,25233-34-5) + 2-Methoxybenzoyl chloride (21615-34-9) → (2-methoxyphenyl)thiophen-2-ylmethanone (6933-34-2)

Guidance literature:

With carbon disulfide; aluminium trichloride;

DOI:10.1021/jo01103a006

upstream raw materials:

thiophene

2-Methoxybenzoyl chloride

(2-hydroxyphenyl)(thiophen-2-yl)methanone

dimethyl sulfate

Downstream raw materials:

(2-methoxyphenyl)(thiophen-2-yl)methanol

(2-methoxyphenyl)(thiophen-2-yl)methanol

1-bromo-2-(5-bromo-[2]thienyl)-2-(2-methoxy-phenyl)-1-phenyl-ethylene

(2-hydroxyphenyl)(thiophen-2-yl)methanone