Cyclotridec[b]indole, dodecahydro-

Base Information

• Chemical Name: Cyclotridec[b]indole, dodecahydro-
• CAS No.: 7140-32-1
• Molecular Formula: C19H27N
• Mol file: 7140-32-1.mol

Synonyms:

Chemical Property of Cyclotridec[b]indole, dodecahydro-

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclotridec[b]indole, dodecahydro-

There total 1 articles about Cyclotridec[b]indole, dodecahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

carbon monoxide (201230-82-2) + cis-cyclododecene (1129-89-1) + phenylhydrazine (100-63-0) → spiro[cyclododecane-1,3'-indoline] + 5,6,7,8,9,10,11,12,13,14,15,16-dodecahydrocyclotridecan[b]indole (7140-32-1)

Guidance literature:

With hydrogen; toluene-4-sulfonic acid; acetylacetonatodicarbonylrhodium(l); In 1,4-dioxane; at 100 ℃; for 24h; under 52504.2 Torr;

DOI:10.1039/b513364e

upstream raw materials:

carbon monoxide

cis-cyclododecene

phenylhydrazine

Refernces