Benzamide, N-(4-ethenylphenyl)-

Base Information

• Chemical Name: Benzamide, N-(4-ethenylphenyl)-
• CAS No.: 7297-64-5
• Molecular Formula: C15H13NO
• Molecular Weight: 223.274
• Mol file: 7297-64-5.mol

Synonyms:

Chemical Property of Benzamide, N-(4-ethenylphenyl)-

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzamide, N-(4-ethenylphenyl)-

There total 4 articles about Benzamide, N-(4-ethenylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

Triethoxyvinylsilane (78-08-0) + N-(4-iodophenyl)benzamide (52807-29-1) → N-(4-vinylphenyl)benzamide (7297-64-5)

Guidance literature:

With tetrabutyl ammonium fluoride; palladium dichloride; In tetrahydrofuran; at 65 ℃; for 9h;

DOI:10.1039/c0nj01019g

Reference yield: 62.0%

4-vinyl benzylamine (1520-21-4,25086-42-4) + benzoyl chloride (98-88-4) → N-(4-vinylphenyl)benzamide (7297-64-5)

Guidance literature:

With triethylamine; In dichloromethane; for 16h; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.9b04413

Reference yield: 58.0%

4-Vinylphenylboronic acid (2156-04-9,593231-72-2) + 3-phenyl-5H-1,4,2-dioxazol-5-one (19226-36-9) → N-(4-vinylphenyl)benzamide (7297-64-5)

Guidance literature:

With water; iron(II) chloride; In 1,2-dichloro-ethane; at 40 ℃; for 24h; Reagent/catalyst; chemoselective reaction; Inert atmosphere; Irradiation;

DOI:10.1021/acscatal.1c04538

upstream raw materials:

4-vinyl benzylamine

benzoyl chloride

4-nitrostyrene

Triethoxyvinylsilane