phenyl N-benzyloxycarbamate

Base Information

Chemical Name:phenyl N-benzyloxycarbamate
CAS No.:730-18-7
Molecular Formula:C14H13NO3
Molecular Weight:243.262
Hs Code.:
DSSTox Substance ID:DTXSID80469939
Nikkaji Number:J2.094.263K
Wikidata:Q82297871

Synonyms:phenyl N-benzyloxycarbamate;Phenyl N-phenylmethoxycarbamate;730-18-7;Carbamic acid, (phenylmethoxy)-, phenyl ester;Phenyl Benzyloxycarbamate;SCHEMBL5696271;DTXSID80469939;XHARTMBSCUKJQJ-UHFFFAOYSA-N;AKOS009024763

Suppliers and Price of phenyl N-benzyloxycarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of phenyl N-benzyloxycarbamate

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:243.08954328
Heavy Atom Count:18
Complexity:245

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CONC(=O)OC2=CC=CC=C2

Technology Process of phenyl N-benzyloxycarbamate

There total 4 articles about phenyl N-benzyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 730-18-7
N-benzyloxycarbamic acid phenyl ester

Guidance literature:: With pyridine; In acetonitrile; 1.) 0 deg C, 2.) 0 deg C - room temperature, 3.) room temperature, 24 h;
DOI:10.1021/ja00375a025

Reference yield: 60.0%

: 622-33-3
N-benzyloxyamine

: 1885-14-9
phenyl chloroformate

: 730-18-7
N-benzyloxycarbamic acid phenyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1039/c7cc07926e

Reference yield:

: 100-44-7
benzyl chloride

: 730-18-7
N-benzyloxycarbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: (i) HONHCO₂Et, KOH, EtOH, (ii) aq. NaOH

2: diethyl ether

In diethyl ether;
DOI:10.1021/jm00316a012